2,3,4-tri-O-benzyl-1-O-(N-tert-butoxycarbonyl-L-phenylalanyl)-L-arabinopyranose, α-anomer

Base Information

Chemical Name:2,3,4-tri-O-benzyl-1-O-(N-tert-butoxycarbonyl-L-phenylalanyl)-L-arabinopyranose, α-anomer
CAS No.:100924-26-3
Molecular Formula:C₄₀H₄₅NO₈
Molecular Weight:667.799
Hs Code.:

Synonyms:2,3,4-tri-O-benzyl-1-O-(N-tert-butoxycarbonyl-L-phenylalanyl)-L-arabinopyranose, α-anomer

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Chemical Property of 2,3,4-tri-O-benzyl-1-O-(N-tert-butoxycarbonyl-L-phenylalanyl)-L-arabinopyranose, α-anomer

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Technology Process of 2,3,4-tri-O-benzyl-1-O-(N-tert-butoxycarbonyl-L-phenylalanyl)-L-arabinopyranose, α-anomer

There total 1 articles about 2,3,4-tri-O-benzyl-1-O-(N-tert-butoxycarbonyl-L-phenylalanyl)-L-arabinopyranose, α-anomer which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 90899-55-1
2,3,4-tri-O-benzyl-β-L-arabinopyranose

: 21148-96-9
N-(tert-butoxycarbonyl)-L-phenylalanine pentachlorophenyl ester

: 100924-27-4
2,3,4-tri-O-benzyl-1-O-(N-tert-butoxycarbonyl-L-phenylalanyl)-L-arabinopyranose, α-anomer

: 100924-26-3
2,3,4-tri-O-benzyl-1-O-(N-tert-butoxycarbonyl-L-phenylalanyl)-L-arabinopyranose, α-anomer

Guidance literature:: With 1H-imidazole; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1016/S0008-6215(00)90456-7

Reference yield: 70.0%

: 100924-26-3
2,3,4-tri-O-benzyl-1-O-(N-tert-butoxycarbonyl-L-phenylalanyl)-L-arabinopyranose, α-anomer

: 100924-30-9
1-O-(N-tert-butoxycarbonyl-L-phenylalanyl)-α-L-arabinopyranose

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate;
DOI:10.1016/S0008-6215(00)90456-7

Reference yield:

: 100924-26-3
2,3,4-tri-O-benzyl-1-O-(N-tert-butoxycarbonyl-L-phenylalanyl)-L-arabinopyranose, α-anomer

: 100924-31-0
2,3,4-tri-O-acetyl-1-O-(N-tert-butoxycarbonyl-L-phenylalanyl)-α-L-arabinopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / H₂ / 10percent Pd/C / ethyl acetate

2: 51 percent / pyridine / 4 h / Ambient temperature

With pyridine; hydrogen; palladium on activated charcoal; In ethyl acetate;
DOI:10.1016/S0008-6215(00)90456-7