Methyl 4-<(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)glyoxyloyl>benzoate

Base Information

Chemical Name:Methyl 4-<(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)glyoxyloyl>benzoate
CAS No.:119436-75-8
Molecular Formula:C₂₄H₂₆O₄
Molecular Weight:378.468
Hs Code.:

Synonyms:Methyl 4-<(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)glyoxyloyl>benzoate

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Chemical Property of Methyl 4-<(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)glyoxyloyl>benzoate

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Technology Process of Methyl 4-<(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)glyoxyloyl>benzoate

There total 5 articles about Methyl 4-<(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)glyoxyloyl>benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.2%

: 102121-54-0
Methyl (E)-4-<2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)ethenyl>benzoate

: 119436-75-8
Methyl 4-<(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)glyoxyloyl>benzoate

Guidance literature:: With selenium(IV) oxide; at 240 ℃; for 5h;
DOI:10.1021/jm00125a027

Reference yield:

: 865-47-4
potassium tert-butylate

: 1253-46-9
4-methoxycarbonylbenzyltriphenylphosphonium bromide

: 104224-50-2
5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphtholyl chloride

: 119436-75-8
Methyl 4-<(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)glyoxyloyl>benzoate

Guidance literature:: With sodium periodate; In ethanol; n-heptane; water; toluene;

Reference yield:

: 6683-48-3
1,1,4,4,6-pentamethyl-1,2,3,4-tetrahydronaphthalene

: 119436-75-8
Methyl 4-<(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenyl)glyoxyloyl>benzoate

Guidance literature:: Multi-step reaction with 4 steps

1: N-bromosuccinimide, azobisisobutyronitrile / CHCl₃

2: benzene / 5 h / Heating

3: NaOMe / methanol

4: 22.2 percent / SeO₂ / 5 h / 240 °C

With N-Bromosuccinimide; selenium(IV) oxide; 2,2'-azobis(isobutyronitrile); sodium methylate; In methanol; chloroform; benzene;
DOI:10.1021/jm00125a027