C₄₃H₅₈N₂O₅

Base Information

Chemical Name:C₄₃H₅₈N₂O₅
CAS No.:1431329-92-8
Molecular Formula:C₄₃H₅₈N₂O₅
Molecular Weight:682.944
Hs Code.:

C<sub>43</sub>H<sub>58</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₄₃H₅₈N₂O₅

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Chemical Property of C₄₃H₅₈N₂O₅

Chemical Property:

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Technology Process of C₄₃H₅₈N₂O₅

There total 17 articles about C₄₃H₅₈N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 140840-85-3
3-(((tert-butyldimethylsilyl)oxy)methyl)cyclopent-2-en-1-one

: 1431329-92-8
C₄₃H₅₈N₂O₅

Guidance literature:: Multi-step reaction with 11 steps

1.1: (S)-DTBM-SEGPHOS; copper(II) acetate monohydrate / toluene / 3 h / 20 °C / Inert atmosphere

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C

2.2: 1 h / -78 - 0 °C

3.1: dichloromethane / 0.5 h / 0 °C

4.1: water; potassium carbonate / 2 h / 0 - 20 °C

5.1: [bis(acetoxy)iodo]benzene; bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]}; magnesium oxide / benzene / 1 h / 60 °C

6.1: triethylamine; dmap / dichloromethane / 1 h / 20 °C

7.1: methanol; potassium carbonate / tetrahydrofuran / 2.25 h / 20 °C

8.1: boron trifluoride diethyl etherate / dichloromethane / 0.75 h / 0 - 20 °C

9.1: water; sodium hydroxide / 1,4-dioxane / 48 h / Reflux

10.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.42 h / -78 °C

10.2: 1.42 h / -78 - 20 °C

11.1: 1-methyl-1H-imidazole / toluene; acetonitrile / 17 h / 80 °C

With 1-methyl-1H-imidazole; methanol; dmap; bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]}; [bis(acetoxy)iodo]benzene; boron trifluoride diethyl etherate; (S)-DTBM-SEGPHOS; water; sodium hexamethyldisilazane; copper(II) acetate monohydrate; magnesium oxide; potassium hexamethylsilazane; potassium carbonate; triethylamine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; toluene; acetonitrile; benzene;
DOI:10.1016/j.tetasy.2013.02.015

Reference yield:

: 1322546-79-1
tert-butyl(dimethyl){[1-(phenylsulfonyl)cyclopent-3-en-1-yl]methoxy}silane

: 1431329-92-8
C₄₃H₅₈N₂O₅

Guidance literature:: Multi-step reaction with 14 steps

1.1: borane-THF / tetrahydrofuran / 1.42 h / 0 °C

1.2: 1 h / 0 °C

2.1: sodium hydrogencarbonate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium bromide; sodium hypochlorite / water; dichloromethane / 1 h / 0 °C

3.1: triethylamine / tetrahydrofuran / 2 h / 50 °C

4.1: (S)-DTBM-SEGPHOS; copper(II) acetate monohydrate / toluene / 3 h / 20 °C / Inert atmosphere

5.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C

5.2: 1 h / -78 - 0 °C

6.1: dichloromethane / 0.5 h / 0 °C

7.1: water; potassium carbonate / 2 h / 0 - 20 °C

8.1: [bis(acetoxy)iodo]benzene; bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]}; magnesium oxide / benzene / 1 h / 60 °C

9.1: triethylamine; dmap / dichloromethane / 1 h / 20 °C

10.1: methanol; potassium carbonate / tetrahydrofuran / 2.25 h / 20 °C

11.1: boron trifluoride diethyl etherate / dichloromethane / 0.75 h / 0 - 20 °C

12.1: water; sodium hydroxide / 1,4-dioxane / 48 h / Reflux

13.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.42 h / -78 °C

13.2: 1.42 h / -78 - 20 °C

14.1: 1-methyl-1H-imidazole / toluene; acetonitrile / 17 h / 80 °C

With 1-methyl-1H-imidazole; methanol; dmap; sodium hypochlorite; borane-THF; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]}; [bis(acetoxy)iodo]benzene; boron trifluoride diethyl etherate; (S)-DTBM-SEGPHOS; water; sodium hexamethyldisilazane; copper(II) acetate monohydrate; magnesium oxide; potassium hexamethylsilazane; sodium hydrogencarbonate; potassium carbonate; triethylamine; potassium bromide; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; toluene; acetonitrile; benzene;
DOI:10.1016/j.tetasy.2013.02.015

Reference yield:

: 1322546-76-8
C₁₂H₁₄O₃S

: 1431329-92-8
C₄₃H₅₈N₂O₅

Guidance literature:: Multi-step reaction with 15 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 15 h / 20 °C

2.1: borane-THF / tetrahydrofuran / 1.42 h / 0 °C

2.2: 1 h / 0 °C

3.1: sodium hydrogencarbonate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium bromide; sodium hypochlorite / water; dichloromethane / 1 h / 0 °C

4.1: triethylamine / tetrahydrofuran / 2 h / 50 °C

5.1: (S)-DTBM-SEGPHOS; copper(II) acetate monohydrate / toluene / 3 h / 20 °C / Inert atmosphere

6.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C

6.2: 1 h / -78 - 0 °C

7.1: dichloromethane / 0.5 h / 0 °C

8.1: water; potassium carbonate / 2 h / 0 - 20 °C

9.1: [bis(acetoxy)iodo]benzene; bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]}; magnesium oxide / benzene / 1 h / 60 °C

10.1: triethylamine; dmap / dichloromethane / 1 h / 20 °C

11.1: methanol; potassium carbonate / tetrahydrofuran / 2.25 h / 20 °C

12.1: boron trifluoride diethyl etherate / dichloromethane / 0.75 h / 0 - 20 °C

13.1: water; sodium hydroxide / 1,4-dioxane / 48 h / Reflux

14.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.42 h / -78 °C

14.2: 1.42 h / -78 - 20 °C

15.1: 1-methyl-1H-imidazole / toluene; acetonitrile / 17 h / 80 °C

With 1H-imidazole; 1-methyl-1H-imidazole; methanol; dmap; sodium hypochlorite; borane-THF; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; bis{rhodium[3,3'-(1,3-phenylene)bis(2,2-dimethylpropanoic acid)]}; [bis(acetoxy)iodo]benzene; boron trifluoride diethyl etherate; (S)-DTBM-SEGPHOS; water; sodium hexamethyldisilazane; copper(II) acetate monohydrate; magnesium oxide; potassium hexamethylsilazane; sodium hydrogencarbonate; potassium carbonate; triethylamine; potassium bromide; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; benzene;
DOI:10.1016/j.tetasy.2013.02.015