C₁₂H₁₇NO₃

Base Information

Chemical Name:C₁₂H₁₇NO₃
CAS No.:1192134-02-3
Molecular Formula:C₁₂H₁₇NO₃
Molecular Weight:223.272
Hs Code.:

C<sub>12</sub>H<sub>17</sub>NO<sub>3</sub>

Synonyms:C₁₂H₁₇NO₃

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Chemical Property of C₁₂H₁₇NO₃

Chemical Property:

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Technology Process of C₁₂H₁₇NO₃

There total 3 articles about C₁₂H₁₇NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1192134-01-2
C₁₂H₁₅NO₅

: 1192134-02-3
C₁₂H₁₇NO₃

Guidance literature:: With hydrogenchloride; iron; acetic acid; In water; ethyl acetate; for 0.25h; Reflux;
DOI:10.1016/j.bmc.2011.07.062

Reference yield:

: 621-59-0
isovanillin

: 1192134-02-3
C₁₂H₁₇NO₃

Guidance literature:: Multi-step reaction with 3 steps

1: nitronium tetrafluoborate / dichloromethane / 24 h / -20 °C / Inert atmosphere

2: caesium carbonate; sodium iodide / N,N-dimethyl-formamide / 25 h / 20 - 80 °C / Inert atmosphere

3: hydrogenchloride; iron; acetic acid / water; ethyl acetate / 0.25 h / Reflux

With hydrogenchloride; nitronium tetrafluoborate; iron; caesium carbonate; acetic acid; sodium iodide; In dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.07.062

Reference yield:

: 6284-92-0
3-hydroxy-4-methoxy-2-nitrobenzaldehyde

: 1192134-02-3
C₁₂H₁₇NO₃

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate; sodium iodide / N,N-dimethyl-formamide / 25 h / 20 - 80 °C / Inert atmosphere

2: hydrogenchloride; iron; acetic acid / water; ethyl acetate / 0.25 h / Reflux

With hydrogenchloride; iron; caesium carbonate; acetic acid; sodium iodide; In water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.07.062