N²,N⁶-dibenzoyl-9-(2',3'-di-O-benzoyl-α-L-threofuranosyl)-2,6-diaminopurine

Base Information

Chemical Name:N²,N⁶-dibenzoyl-9-(2',3'-di-O-benzoyl-α-L-threofuranosyl)-2,6-diaminopurine
CAS No.:425394-07-6
Molecular Formula:C₃₇H₂₈N₆O₇
Molecular Weight:668.665
Hs Code.:

N<sup>2</sup>,N<sup>6</sup>-dibenzoyl-9-(2',3'-di-O-benzoyl-α-L-threofuranosyl)-2,6-diaminopurine

Synonyms:N²,N⁶-dibenzoyl-9-(2',3'-di-O-benzoyl-α-L-threofuranosyl)-2,6-diaminopurine

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Chemical Property of N²,N⁶-dibenzoyl-9-(2',3'-di-O-benzoyl-α-L-threofuranosyl)-2,6-diaminopurine

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Technology Process of N²,N⁶-dibenzoyl-9-(2',3'-di-O-benzoyl-α-L-threofuranosyl)-2,6-diaminopurine

There total 4 articles about N²,N⁶-dibenzoyl-9-(2',3'-di-O-benzoyl-α-L-threofuranosyl)-2,6-diaminopurine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.1%

: 51173-57-0
2,6-diaminopurine-N²,N⁶-dibenzoate

: 325683-77-0
1-O-acetyl-2,3-di-O-benzoyl-L-threofuranose

: 425394-07-6
N²,N⁶-dibenzoyl-9-(2',3'-di-O-benzoyl-α-L-threofuranosyl)-2,6-diaminopurine

Guidance literature:: With benzenesulfonamide; trimethyl((trifluoromethyl)sulfonyl)silane; In acetonitrile; at 65 ℃; for 3h;
DOI:10.1002/hlca.200290000

Reference yield: 59.0%

: 51173-57-0
2,6-diaminopurine-N²,N⁶-dibenzoate

: C₂₀H₁₈O₇

: 425394-07-6
N²,N⁶-dibenzoyl-9-(2',3'-di-O-benzoyl-α-L-threofuranosyl)-2,6-diaminopurine

Guidance literature:: With benzenesulfonamide; trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 65 ℃; for 3h;
DOI:10.1021/ol020016p

Reference yield:

: 538368-86-4
2′,3′-di-O-benzoyl-L-threonolactone

: 425394-07-6
N²,N⁶-dibenzoyl-9-(2',3'-di-O-benzoyl-α-L-threofuranosyl)-2,6-diaminopurine

Guidance literature:: Multi-step reaction with 3 steps

1: 53 percent / DIBAL-H / toluene / -78 °C

2: 93 percent / DMAP; pyridine / CH₂Cl₂ / 18 h / 20 °C

3: 59.1 percent / BSA; TMS-Tf / acetonitrile / 3 h / 65 °C

With pyridine; benzenesulfonamide; dmap; diisobutylaluminium hydride; trimethyl((trifluoromethyl)sulfonyl)silane; In dichloromethane; toluene; acetonitrile;
DOI:10.1002/hlca.200290000