((phenyl)vinylacetato)(carbonyl)(η-1-acetone)bis(triisopropylphosphine)ruthenium(II) tetrafluoroborate

Base Information

Chemical Name:((phenyl)vinylacetato)(carbonyl)(η-1-acetone)bis(triisopropylphosphine)ruthenium(II) tetrafluoroborate
CAS No.:155917-08-1
Molecular Formula:BF₄*C₃₂H₅₇O₄P₂Ru
Molecular Weight:755.624
Hs Code.:

Synonyms:((phenyl)vinylacetato)(carbonyl)(η-1-acetone)bis(triisopropylphosphine)ruthenium(II) tetrafluoroborate

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Chemical Property of ((phenyl)vinylacetato)(carbonyl)(η-1-acetone)bis(triisopropylphosphine)ruthenium(II) tetrafluoroborate

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Technology Process of ((phenyl)vinylacetato)(carbonyl)(η-1-acetone)bis(triisopropylphosphine)ruthenium(II) tetrafluoroborate

There total 2 articles about ((phenyl)vinylacetato)(carbonyl)(η-1-acetone)bis(triisopropylphosphine)ruthenium(II) tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: tetrafluoroboric acid

: 155941-30-3
(phenylethynyl)(η2-acetato)(carbonyl)bis(triisopropylphosphine)ruthenium(II)

: 155917-08-1
((phenyl)vinylacetato)(carbonyl)(η-1-acetone)bis(triisopropylphosphine)ruthenium(II) tetrafluoroborate

Guidance literature:: With CH₃COOH; (CH₃)2CO; In diethyl ether; acetone; under Ar, standard Schlenk techniques; treating a soln. of Ru-compd. inacetone with an Et2O soln. of HBF4, stirring for 1 h at room temp.; concg. of soln. until pptn., completion of pptn. by addn. of Et2O, filtering off the ppt., washing with Et2O and drying in vac.; elem. anal.;
DOI:10.1021/om00017a026

Reference yield:

: tetrafluoroboric acid

: 155917-12-7
(phenylethynyl)((phenyl)vinylacetato)(carbonyl)bis(triisopropylphosphine)ruthenium(II)

: 155917-08-1
((phenyl)vinylacetato)(carbonyl)(η-1-acetone)bis(triisopropylphosphine)ruthenium(II) tetrafluoroborate

Guidance literature:: With (CH₃)2CO; byproducts: (C6H5)CCH;
DOI:10.1021/om00017a026

Reference yield: 86.0%

: 155917-08-1
((phenyl)vinylacetato)(carbonyl)(η-1-acetone)bis(triisopropylphosphine)ruthenium(II) tetrafluoroborate

: 155917-31-0
((phenyl)vinylacetato)(carbonyl)(acetonitrile)bis(triisopropylphosphine)ruthenium(II) tetrafluoroborate

Guidance literature:: With CH₃CN; In acetonitrile; byproducts: (CH3)2CO; under Ar, standard Schlenk techniques; dissolving of Ru-compd. in CH3CN; pptn. by addn. of Et2O;
DOI:10.1021/om00017a026