(chloro)((phenyl)vinylacetato)(carbonyl)bis(triisopropylphosphine)ruthenium(II)

Base Information

Chemical Name:(chloro)((phenyl)vinylacetato)(carbonyl)bis(triisopropylphosphine)ruthenium(II)
CAS No.:155917-13-8
Molecular Formula:C₂₉H₅₁ClO₃P₂Ru
Molecular Weight:646.193
Hs Code.:

Synonyms:(chloro)((phenyl)vinylacetato)(carbonyl)bis(triisopropylphosphine)ruthenium(II)

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Chemical Property of (chloro)((phenyl)vinylacetato)(carbonyl)bis(triisopropylphosphine)ruthenium(II)

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Technology Process of (chloro)((phenyl)vinylacetato)(carbonyl)bis(triisopropylphosphine)ruthenium(II)

There total 1 articles about (chloro)((phenyl)vinylacetato)(carbonyl)bis(triisopropylphosphine)ruthenium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 155917-08-1
((phenyl)vinylacetato)(carbonyl)(η-1-acetone)bis(triisopropylphosphine)ruthenium(II) tetrafluoroborate

: 155917-13-8
(chloro)((phenyl)vinylacetato)(carbonyl)bis(triisopropylphosphine)ruthenium(II)

Guidance literature:: With NaCl; In methanol; byproducts: NaBF4, (CH3)2CO; under Ar, standard Schlenk techniques; treating a soln. of Ru-compd. inMeOH with NaCl, stirring for 2 h at room temp.; filtering off the ppt., washing with MeOH and drying in vac.; elem. anal.;
DOI:10.1021/om00017a026

Reference yield: 55.0%

: tetrafluoroboric acid

: 155917-13-8
(chloro)((phenyl)vinylacetato)(carbonyl)bis(triisopropylphosphine)ruthenium(II)

: 155917-15-0
(chloro)(CCH₂(phenyl)acetato)(carbonyl)bis(triisopropylphosphine)ruthenium(II) tetrafluoroborate

Guidance literature:: In methanol; under Ar, standard Schlenk techniques; treating a soln. of Ru-compd. inCH2Cl2 with HBF4 in Et2O, stirring for 20 min at room temp.; concg. of soln., pptn. by addn. of Et2O, filtering off the ppt., washing with MeOH and drying in vac.; elem. anal.;
DOI:10.1021/om00017a026