C₂₄H₄₂N₂O₆Si

Base Information

Chemical Name:C₂₄H₄₂N₂O₆Si
CAS No.:608136-36-3
Molecular Formula:C₂₄H₄₂N₂O₆Si
Molecular Weight:482.693
Hs Code.:

C<sub>24</sub>H<sub>42</sub>N<sub>2</sub>O<sub>6</sub>Si

Synonyms:C₂₄H₄₂N₂O₆Si

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Chemical Property of C₂₄H₄₂N₂O₆Si

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Technology Process of C₂₄H₄₂N₂O₆Si

There total 7 articles about C₂₄H₄₂N₂O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 608136-35-2
C₂₆H₄₄N₂O₇Si

: 608136-36-3
C₂₄H₄₂N₂O₆Si

Guidance literature:: With water; potassium carbonate; In methanol; at 20 ℃; for 6h;
DOI:10.1021/jo034441n

Reference yield:

: 608136-23-8
(S)-5-benzyloxy-1-tert-butyldimethylsilyloxy-2-pentanol

: 608136-36-3
C₂₄H₄₂N₂O₆Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: 92 percent / DMAP; pyridine / CHCl₃ / 0 - 20 °C

2.1: 95 percent / H₂ / Pd/C / methanol / 0.5 h / 20 °C / 760 Torr

3.1: 100 percent / Dess-Martin periodinane / CHCl₃ / 0 - 20 °C

4.1: methanol / 0 - 20 °C

4.2: 58 percent / acetic acid; sodium cyanoborohydride / methanol / 0 - 20 °C

5.1: 98 percent / aqueous sodium bicarbonate / CHCl₃ / 1.5 h / 0 °C

6.1: 64 percent / H₂O; K₂CO₃ / methanol / 6 h / 20 °C

With pyridine; dmap; water; hydrogen; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; palladium on activated charcoal; In methanol; chloroform; 3.1: Dess-Martin oxidation;
DOI:10.1021/jo034441n

Reference yield:

: 608136-24-9
(S)-2-acetoxy-5-benzyloxy-1-(tert-butyldimethylsilyloxy)pentane

: 608136-36-3
C₂₄H₄₂N₂O₆Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: 95 percent / H₂ / Pd/C / methanol / 0.5 h / 20 °C / 760 Torr

2.1: 100 percent / Dess-Martin periodinane / CHCl₃ / 0 - 20 °C

3.1: methanol / 0 - 20 °C

3.2: 58 percent / acetic acid; sodium cyanoborohydride / methanol / 0 - 20 °C

4.1: 98 percent / aqueous sodium bicarbonate / CHCl₃ / 1.5 h / 0 °C

5.1: 64 percent / H₂O; K₂CO₃ / methanol / 6 h / 20 °C

With water; hydrogen; sodium hydrogencarbonate; potassium carbonate; Dess-Martin periodane; palladium on activated charcoal; In methanol; chloroform; 2.1: Dess-Martin oxidation;
DOI:10.1021/jo034441n