Technology Process of C17H26O4
There total 1 articles about C17H26O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 6h;
DOI:10.1055/s-2007-982556
- Guidance literature:
-
With
sodium hydride;
In
tetrahydrofuran;
at 20 ℃;
for 12h;
DOI:10.1055/s-2007-982556
- Guidance literature:
-
Multi-step reaction with 8 steps
1: NaH / tetrahydrofuran / 12 h / 20 °C
2: acetic acid; water / 15 h / 55 °C
3: 100 percent / pyridinium chlorochromate; NaOAc / 3 h / 20 °C
4: 95 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 12 h / 20 °C
5: 90 percent / n-BuLi / tetrahydrofuran / 1.5 h / -78 °C
6: 85 percent / triethyl silane; boron trifluoride*diethyl ether / CH2Cl2; acetonitrile / 2 h / -40 °C
7: 70 percent / mercury(II) oxide; aqueous sulfuric acid / acetone / 1 h / 50 °C
8: NaHMDS / tetrahydrofuran / 4 h / -78 - 20 °C
With
triethylsilane; n-butyllithium; sulfuric acid; boron trifluoride diethyl etherate; water; sodium acetate; sodium hexamethyldisilazane; sodium hydride; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; pyridinium chlorochromate; mercury(II) oxide;
In
tetrahydrofuran; dichloromethane; acetone; acetonitrile;
DOI:10.1055/s-2007-982556