C₁₃H₁₆F₂O₆

Base Information

Chemical Name:C₁₃H₁₆F₂O₆
CAS No.:1413374-46-5
Molecular Formula:C₁₃H₁₆F₂O₆
Molecular Weight:306.263
Hs Code.:

C<sub>13</sub>H<sub>16</sub>F<sub>2</sub>O<sub>6</sub>

Synonyms:C₁₃H₁₆F₂O₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₆F₂O₆

Chemical Property:

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Technology Process of C₁₃H₁₆F₂O₆

There total 21 articles about C₁₃H₁₆F₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1413374-43-2
C₄₈H₄₆F₂O₆

: 1413374-46-5
C₁₃H₁₆F₂O₆

Guidance literature:: With hydrogenchloride; hydrogen; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; at 20 ℃; for 72h;

Reference yield:

: 4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9
2,3,4,6-Tetra-O-benzyl-D-glucopyranose

: 1413374-46-5
C₁₃H₁₆F₂O₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: toluene; tetrahydrofuran / 3.67 h / 0 - 50 °C / Inert atmosphere

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.25 h / -78 - -40 °C / Inert atmosphere

2.2: 2.25 h / -78 - 20 °C

3.1: L-proline / dimethyl sulfoxide / 8 h / 50 °C

4.1: pyridine; trichlorophosphate / 0 - 20 °C

5.1: cerium(III) chloride heptahydrate / tetrahydrofuran; methanol / 0.5 h / -23 °C

5.2: 0.75 h

6.1: phosphorus pentoxide / chloroform / 1 h / 20 °C / Inert atmosphere

7.1: sodium methylate; methanol / 20 °C / Industry scale

8.1: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

9.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C

9.2: 0 - 50 °C

10.1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / ethanol; tetrahydrofuran / 72 h / 20 °C

With pyridine; hydrogenchloride; methanol; oxalyl dichloride; phosphorus pentoxide; cerium(III) chloride heptahydrate; hydrogen; sodium methylate; sodium hydride; dimethyl sulfoxide; L-proline; trichlorophosphate; palladium 10% on activated carbon; In tetrahydrofuran; methanol; ethanol; dichloromethane; chloroform; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; mineral oil;

Reference yield:

: 110391-10-1
(4R,5S,6R)-4,5,6-tris(benzyloxy)-3-((benzyloxy)methyl)-2-cyclohexen-1-one

: 1413374-46-5
C₁₃H₁₆F₂O₆

Guidance literature:: Multi-step reaction with 11 steps

1.1: cerium(III) chloride heptahydrate / tetrahydrofuran; methanol / 0.5 h / -23 °C

1.2: 0.75 h

2.1: 1H-imidazole / N,N-dimethyl-formamide / 0.5 h / 20 °C / Inert atmosphere

2.2: 12 h / 40 °C

3.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

3.2: 2 h / 0 - 20 °C

4.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C / Inert atmosphere

5.1: hydrogenchloride; methanol / dichloromethane / 20 °C

6.1: pyridine / dmap / dichloromethane / 0.75 h / 0 °C / Inert atmosphere

7.1: diethylamino-sulfur trifluoride / dichloromethane / 16 h / 20 °C / Inert atmosphere

8.1: sodium methylate; methanol / 20 °C / Industry scale

9.1: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

10.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C

10.2: 0 - 50 °C

11.1: hydrogenchloride; hydrogen / palladium 10% on activated carbon / ethanol; tetrahydrofuran / 72 h / 20 °C

With pyridine; 1H-imidazole; hydrogenchloride; methanol; diethylamino-sulfur trifluoride; cerium(III) chloride heptahydrate; dimethylsulfide borane complex; hydrogen; sodium methylate; sodium hydride; Dess-Martin periodane; dmap; palladium 10% on activated carbon; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; mineral oil;