Succinic acid benzyl ester (2R,3R,4R,5R,6R)-3,4-diacetoxy-5-acetylamino-6-[6-(9H-fluoren-9-ylmethoxycarbonylamino)-hexyloxy]-tetrahydro-pyran-2-ylmethyl ester

Base Information

Chemical Name:Succinic acid benzyl ester (2R,3R,4R,5R,6R)-3,4-diacetoxy-5-acetylamino-6-[6-(9H-fluoren-9-ylmethoxycarbonylamino)-hexyloxy]-tetrahydro-pyran-2-ylmethyl ester
CAS No.:290308-58-6
Molecular Formula:C₄₄H₅₂N₂O₁₃
Molecular Weight:816.902
Hs Code.:

Succinic acid benzyl ester (2R,3R,4R,5R,6R)-3,4-diacetoxy-5-acetylamino-6-[6-(9H-fluoren-9-ylmethoxycarbonylamino)-hexyloxy]-tetrahydro-pyran-2-ylmethyl ester

Synonyms:Succinic acid benzyl ester (2R,3R,4R,5R,6R)-3,4-diacetoxy-5-acetylamino-6-[6-(9H-fluoren-9-ylmethoxycarbonylamino)-hexyloxy]-tetrahydro-pyran-2-ylmethyl ester

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Chemical Property of Succinic acid benzyl ester (2R,3R,4R,5R,6R)-3,4-diacetoxy-5-acetylamino-6-[6-(9H-fluoren-9-ylmethoxycarbonylamino)-hexyloxy]-tetrahydro-pyran-2-ylmethyl ester

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Technology Process of Succinic acid benzyl ester (2R,3R,4R,5R,6R)-3,4-diacetoxy-5-acetylamino-6-[6-(9H-fluoren-9-ylmethoxycarbonylamino)-hexyloxy]-tetrahydro-pyran-2-ylmethyl ester

There total 2 articles about Succinic acid benzyl ester (2R,3R,4R,5R,6R)-3,4-diacetoxy-5-acetylamino-6-[6-(9H-fluoren-9-ylmethoxycarbonylamino)-hexyloxy]-tetrahydro-pyran-2-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 127903-20-2
9H-fluoren-9-ylmethyl N-(6-hydroxyhexyl)carbamate

: 290308-57-5
Succinic acid benzyl ester (2R,3R,4R,5R,6R)-3,4,6-triacetoxy-5-acetylamino-tetrahydro-pyran-2-ylmethyl ester

: 290308-58-6
Succinic acid benzyl ester (2R,3R,4R,5R,6R)-3,4-diacetoxy-5-acetylamino-6-[6-(9H-fluoren-9-ylmethoxycarbonylamino)-hexyloxy]-tetrahydro-pyran-2-ylmethyl ester

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 45 ℃; for 16h;

Reference yield:

: Succinic acid benzyl ester (2R,3R,4R,5R,6R)-4,6-diacetoxy-5-acetylamino-3-hydroxy-tetrahydro-pyran-2-ylmethyl ester

: 290308-58-6
Succinic acid benzyl ester (2R,3R,4R,5R,6R)-3,4-diacetoxy-5-acetylamino-6-[6-(9H-fluoren-9-ylmethoxycarbonylamino)-hexyloxy]-tetrahydro-pyran-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine

2: 80 percent / Me₃Si-triflate / 1,2-dichloro-ethane / 16 h / 45 °C

With pyridine; trimethylsilyl trifluoromethanesulfonate; In 1,2-dichloro-ethane; 1: Acetylation / 2: Substitution;