C₄₆H₅₅ClN₄O₁₆

Base Information

Chemical Name:C₄₆H₅₅ClN₄O₁₆
CAS No.:223572-34-7
Molecular Formula:C₄₆H₅₅ClN₄O₁₆
Molecular Weight:955.413
Hs Code.:

C<sub>46</sub>H<sub>55</sub>ClN<sub>4</sub>O<sub>16</sub>

Synonyms:C₄₆H₅₅ClN₄O₁₆

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Chemical Property of C₄₆H₅₅ClN₄O₁₆

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Technology Process of C₄₆H₅₅ClN₄O₁₆

There total 10 articles about C₄₆H₅₅ClN₄O₁₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 223572-42-7
C₅₄H₆₁ClN₄O₁₈

: 223572-34-7
C₄₆H₅₅ClN₄O₁₆

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; ethyl acetate; at 25 ℃; for 7.5h;
DOI:10.1021/ja990189i

Reference yield:

: 223572-32-5
C₂₂H₃₀BNO₉

: 223572-34-7
C₄₆H₅₅ClN₄O₁₆

Guidance literature:: Multi-step reaction with 4 steps

1: Pd₂(dba)3; (o-tolyl)3P; 1 N aq. Na₂CO₃ / methanol; toluene / 0.25 h / 80 °C

2: 96 percent / Bu₄NF; AcOH / tetrahydrofuran / 6 h / 25 °C

3: 99 percent / 0.2 N aq. LiOH / tetrahydrofuran / 1 h / 0 °C

4: 80 percent / H₂ / 10 percent Pd/C / ethanol; ethyl acetate / 11 h / 25 °C

With lithium hydroxide; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; tetrabutyl ammonium fluoride; hydrogen; sodium carbonate; acetic acid; tris-(o-tolyl)phosphine; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; ethyl acetate; toluene; 1: Suzuki coupling / 2: desilylation / 3: Hydrolysis / 4: Hydrogenolysis;
DOI:10.1021/ja992577q

Reference yield:

: 223572-33-6
C₆₁H₇₇ClN₄O₁₈Si

: 223572-34-7
C₄₆H₅₅ClN₄O₁₆

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / Bu₄NF; AcOH / tetrahydrofuran / 6 h / 25 °C

2: 99 percent / 0.2 N aq. LiOH / tetrahydrofuran / 1 h / 0 °C

3: 80 percent / H₂ / 10 percent Pd/C / ethanol; ethyl acetate / 11 h / 25 °C

With lithium hydroxide; tetrabutyl ammonium fluoride; hydrogen; acetic acid; palladium on activated charcoal; In tetrahydrofuran; ethanol; ethyl acetate; 1: desilylation / 2: Hydrolysis / 3: Hydrogenolysis;
DOI:10.1021/ja992577q