(3S,4S)-N-<2-(dimethylamino)ethyl>-3,4-bispyrrolidine

Base Information

Chemical Name:(3S,4S)-N-<2-(dimethylamino)ethyl>-3,4-bispyrrolidine
CAS No.:87974-34-3
Molecular Formula:C₃₆H₄₄N₂O₆P₂
Molecular Weight:662.703
Hs Code.:

(3S,4S)-N-<2-(dimethylamino)ethyl>-3,4-bis<bis(4-methoxyphenyl)phosphinooxy>pyrrolidine

Synonyms:(3S,4S)-N-<2-(dimethylamino)ethyl>-3,4-bispyrrolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,4S)-N-<2-(dimethylamino)ethyl>-3,4-bispyrrolidine

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Technology Process of (3S,4S)-N-<2-(dimethylamino)ethyl>-3,4-bispyrrolidine

There total 1 articles about (3S,4S)-N-<2-(dimethylamino)ethyl>-3,4-bispyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 13685-30-8
chlorobis(4-methoxyphenyl)phosphane

: 87974-36-5
(3S,4S)-1-<2-(Dimethylamino)ethyl>-3,4-pyrrolidinediol

: 87974-34-3
(3S,4S)-N-<2-(dimethylamino)ethyl>-3,4-bispyrrolidine

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 ℃; for 0.5h; reaction repeated with crude product;
DOI:10.1246/bcsj.57.739

Reference yield: 48.0%

: rhodium(I)-bis(1,5-cyclooctadiene) tetrafluoroborate

: 87974-34-3
(3S,4S)-N-<2-(dimethylamino)ethyl>-3,4-bispyrrolidine

: [Rh((CH₃)2NHCH₂CH₂N(CH₂CHOP(C₆H₄OCH₃)2)2)(C₈H₁₂)]⁽²⁺⁾*BF₄^(1-)*ClO₄^(1-)

Guidance literature:: With perchloric acid; In methanol; ethanol; to soln. of reagents in EtOH-MeOH HClO4 added as EtOH soln., stirred for 15 min at room temp; concd., crystals filtered under N2, dried in vac.;
DOI:10.1246/bcsj.57.823