methyl N-{4-[4-(thiazol-2-ylsulfonylamino)phenylcarbamoyl]phenyl}-p-aminocarbonylbenzoate

Base Information

Chemical Name:methyl N-{4-[4-(thiazol-2-ylsulfonylamino)phenylcarbamoyl]phenyl}-p-aminocarbonylbenzoate
CAS No.:1369424-12-3
Molecular Formula:C₂₅H₂₀N₄O₆S₂
Molecular Weight:536.589
Hs Code.:

Synonyms:methyl N-{4-[4-(thiazol-2-ylsulfonylamino)phenylcarbamoyl]phenyl}-p-aminocarbonylbenzoate

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Chemical Property of methyl N-{4-[4-(thiazol-2-ylsulfonylamino)phenylcarbamoyl]phenyl}-p-aminocarbonylbenzoate

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Technology Process of methyl N-{4-[4-(thiazol-2-ylsulfonylamino)phenylcarbamoyl]phenyl}-p-aminocarbonylbenzoate

There total 5 articles about methyl N-{4-[4-(thiazol-2-ylsulfonylamino)phenylcarbamoyl]phenyl}-p-aminocarbonylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.1%

: 72-14-0
Sulfathiazole

: 1369424-71-4
4-(4-(methoxycarbonyl)benzoylamino)benzoyl chloride

: 1369424-12-3
methyl N-{4-[4-(thiazol-2-ylsulfonylamino)phenylcarbamoyl]phenyl}-p-aminocarbonylbenzoate

Guidance literature:: With pyridine; In acetone; at 20 ℃;
DOI:10.1016/j.bmcl.2013.02.073

Reference yield:

: 7377-26-6
4-Methoxycarbonylbenzoyl chloride

: 1369424-12-3
methyl N-{4-[4-(thiazol-2-ylsulfonylamino)phenylcarbamoyl]phenyl}-p-aminocarbonylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / tetrahydrofuran / 12 h / 20 °C

2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 20 °C

3: pyridine / acetone / 20 °C

With pyridine; oxalyl dichloride; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1016/j.bmcl.2013.02.073

Reference yield:

: 150-13-0,159246-81-8,8014-65-1
4-amino-benzoic acid

: 1369424-12-3
methyl N-{4-[4-(thiazol-2-ylsulfonylamino)phenylcarbamoyl]phenyl}-p-aminocarbonylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / tetrahydrofuran / 12 h / 20 °C

2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 20 °C

3: pyridine / acetone / 20 °C

With pyridine; oxalyl dichloride; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane; acetone;
DOI:10.1016/j.bmcl.2013.02.073