(Z)-methyl-4-((5-(4-methoxyphenyl)-1H-pyrrole-2-yl) (5-(4-methoxyphenyl)-2H-pyrrole-2-ylidene)methyl)benzoate

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Chemical Name:(Z)-methyl-4-((5-(4-methoxyphenyl)-1H-pyrrole-2-yl) (5-(4-methoxyphenyl)-2H-pyrrole-2-ylidene)methyl)benzoate
CAS No.:1363512-35-9
Molecular Formula:C₃₁H₂₆N₂O₄
Molecular Weight:490.558
Hs Code.:

Synonyms:(Z)-methyl-4-((5-(4-methoxyphenyl)-1H-pyrrole-2-yl) (5-(4-methoxyphenyl)-2H-pyrrole-2-ylidene)methyl)benzoate

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Chemical Property of (Z)-methyl-4-((5-(4-methoxyphenyl)-1H-pyrrole-2-yl) (5-(4-methoxyphenyl)-2H-pyrrole-2-ylidene)methyl)benzoate

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Technology Process of (Z)-methyl-4-((5-(4-methoxyphenyl)-1H-pyrrole-2-yl) (5-(4-methoxyphenyl)-2H-pyrrole-2-ylidene)methyl)benzoate

There total 3 articles about (Z)-methyl-4-((5-(4-methoxyphenyl)-1H-pyrrole-2-yl) (5-(4-methoxyphenyl)-2H-pyrrole-2-ylidene)methyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 23.0%

: 1363512-34-8
methyl 4-(bis(5-(4-methoxyphenyl)-1H-pyrrole-2-yl)methyl)-benzoate

: 1363512-35-9
(Z)-methyl-4-((5-(4-methoxyphenyl)-1H-pyrrole-2-yl) (5-(4-methoxyphenyl)-2H-pyrrole-2-ylidene)methyl)benzoate

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1039/c2cc30569k

Reference yield:

: 637354-46-2
2-(4-methoxyphenyl)-1-tosyl-1H-pyrrole

: 1363512-35-9
(Z)-methyl-4-((5-(4-methoxyphenyl)-1H-pyrrole-2-yl) (5-(4-methoxyphenyl)-2H-pyrrole-2-ylidene)methyl)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / ethanol / 3 h / Reflux

2: trifluoroacetic acid / ethyl acetate / 1 h / 20 °C / Inert atmosphere

3: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 20 °C

With trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; In ethanol; dichloromethane; ethyl acetate;
DOI:10.1039/c2cc30569k

Reference yield:

: 4995-12-4
2-(4-methoxyphenyl)-1H-pyrrole

: 1363512-35-9
(Z)-methyl-4-((5-(4-methoxyphenyl)-1H-pyrrole-2-yl) (5-(4-methoxyphenyl)-2H-pyrrole-2-ylidene)methyl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / ethyl acetate / 1 h / 20 °C / Inert atmosphere

2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 20 °C

With trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; ethyl acetate;
DOI:10.1039/c2cc30569k