benzyl N-[trans-2-(2'-acetylaminocyclohexyloxy)acetyl]-L-alanyl-D-isoglutaminate

Base Information

• Chemical Name: benzyl N-[trans-2-(2'-acetylaminocyclohexyloxy)acetyl]-L-alanyl-D-isoglutaminate
• CAS No.: 142034-85-3
• Molecular Formula: C₂₅H₃₆N₄O₇
• Molecular Weight: 504.583

Synonyms:benzyl N-[trans-2-(2'-acetylaminocyclohexyloxy)acetyl]-L-alanyl-D-isoglutaminate

Chemical Property of benzyl N-[trans-2-(2'-acetylaminocyclohexyloxy)acetyl]-L-alanyl-D-isoglutaminate

Chemical Property:

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Technology Process of benzyl N-[trans-2-(2'-acetylaminocyclohexyloxy)acetyl]-L-alanyl-D-isoglutaminate

There total 17 articles about benzyl N-[trans-2-(2'-acetylaminocyclohexyloxy)acetyl]-L-alanyl-D-isoglutaminate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

L-alanyl-D-glutamine benzyl ester hydrochloride (128753-64-0) + (1'S,2'S)-2-(2'-Acetylaminocyclohexyloxy)acetic acid (142034-82-0) → (1'S,2'S)-Benzyl-N-<2-(2'-acetylaminocyclohexyloxy)acetyl>-L-alanyl-D-isoglutaminate (141949-62-4,142034-85-3,142034-86-4)

Guidance literature:

With diphenylphosphoranyl azide; triethylamine; In N,N-dimethyl-formamide; a) 0-2 deg C, 1 h, b) r.t., 60 h;

DOI:10.1016/S0040-4020(01)90182-6

Reference yield: 0.215%

L-alanyl-D-glutamine benzyl ester hydrochloride (128753-64-0) + trans-2-(2'-acetylaminocyclohexyloxy)acetic acid (134961-98-1,142034-81-9,142034-82-0,144409-23-4) → (1'S,2'S)-Benzyl-N-<2-(2'-acetylaminocyclohexyloxy)acetyl>-L-alanyl-D-isoglutaminate (141949-62-4,142034-85-3,142034-86-4) + (1'R,2'R)-Benzyl-N-<2-(2'-acetylaminocyclohexyloxy)acetyl>-L-alanyl-D-isoglutaminate (141949-62-4,142034-85-3,142034-86-4)

Guidance literature:

With diphenylphosphoranyl azide; triethylamine; In N,N-dimethyl-formamide; a) 0-2 deg C, 1 h, b) r.t., 60 h;

DOI:10.1016/S0040-4020(01)90182-6

Reference yield: 0.215%

L-alanyl-D-glutamine benzyl ester hydrochloride (128753-64-0) + trans-2-(2'-acetylaminocyclohexyloxy)acetic acid (134961-98-1,142034-81-9,142034-82-0,144409-23-4) → (1'S,2'S)-Benzyl-N-<2-(2'-acetylaminocyclohexyloxy)acetyl>-L-alanyl-D-isoglutaminate (141949-62-4,142034-85-3,142034-86-4) + (1'R,2'R)-Benzyl-N-<2-(2'-acetylaminocyclohexyloxy)acetyl>-L-alanyl-D-isoglutaminate (141949-62-4,142034-85-3,142034-86-4)

Guidance literature:

With diphenylphosphoranyl azide; triethylamine; In N,N-dimethyl-formamide; a) 0-2 deg C, 1 h, b) r.t., 60 h;

DOI:10.1016/S0040-4020(01)90182-6

upstream raw materials:

L-alanyl-D-glutamine benzyl ester hydrochloride

trans-2-(2'-acetylaminocyclohexyloxy)acetic acid

(1'S,2'S)-2-(2'-Acetylaminocyclohexyloxy)acetic acid

(1S,2S)-trans-2-aminocyclohexanol

Downstream raw materials:

(1'R,2'R)-N-<2-(2'-Acetylaminocyclohexyloxy)acetyl>-L-alanyl-D-isoglutamine

(1'S,2'S)-N-<2-(2'-Acetylaminocyclohexyloxy)acetyl>-L-alanyl-D-isoglutamine

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