(8S,9R,11S,13S,14S)-11-(4-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)phenyl)-7,8,9,11,12,13,15,16-octahydro-3-hydroxy-13-methyl-6hcyclopenta[a]phenanthren-17(14H)-one

Base Information

Chemical Name:(8S,9R,11S,13S,14S)-11-(4-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)phenyl)-7,8,9,11,12,13,15,16-octahydro-3-hydroxy-13-methyl-6hcyclopenta[a]phenanthren-17(14H)-one
CAS No.:1236152-98-9
Molecular Formula:C₃₀H₃₇N₃O₅
Molecular Weight:519.641
Hs Code.:

(8S,9R,11S,13S,14S)-11-(4-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)phenyl)-7,8,9,11,12,13,15,16-octahydro-3-hydroxy-13-methyl-6hcyclopenta[a]phenanthren-17(14H)-one

Synonyms:(8S,9R,11S,13S,14S)-11-(4-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)phenyl)-7,8,9,11,12,13,15,16-octahydro-3-hydroxy-13-methyl-6hcyclopenta[a]phenanthren-17(14H)-one

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Chemical Property of (8S,9R,11S,13S,14S)-11-(4-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)phenyl)-7,8,9,11,12,13,15,16-octahydro-3-hydroxy-13-methyl-6hcyclopenta[a]phenanthren-17(14H)-one

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Technology Process of (8S,9R,11S,13S,14S)-11-(4-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)phenyl)-7,8,9,11,12,13,15,16-octahydro-3-hydroxy-13-methyl-6hcyclopenta[a]phenanthren-17(14H)-one

There total 9 articles about (8S,9R,11S,13S,14S)-11-(4-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)phenyl)-7,8,9,11,12,13,15,16-octahydro-3-hydroxy-13-methyl-6hcyclopenta[a]phenanthren-17(14H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19249-03-7
triethylene glycol di-(p-toluenesulfonate)

: 1236152-98-9
(8S,9R,11S,13S,14S)-11-(4-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)phenyl)-7,8,9,11,12,13,15,16-octahydro-3-hydroxy-13-methyl-6hcyclopenta[a]phenanthren-17(14H)-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium azide / ethanol / 2 h / Reflux

2.1: potassium carbonate / acetonitrile / 0.08 h

2.2: 10 h / 80 °C

3.1: potassium hydroxide / methanol; hexane

With sodium azide; potassium carbonate; potassium hydroxide; In methanol; ethanol; hexane; acetonitrile; 2.2: Williamson synthesis;
DOI:10.1016/j.bmc.2012.04.041

Reference yield:

: 1236153-00-6
(8S,9R,11S,13S,14S)-11-(4-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)phenyl)-7,8,9,11,12,13,14,15,16,17-decahydro-13-methyl-17-oxo-6H-cyclopenta[a]phenanthren-3-yl acetate

: 1236152-98-9
(8S,9R,11S,13S,14S)-11-(4-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)phenyl)-7,8,9,11,12,13,15,16-octahydro-3-hydroxy-13-methyl-6hcyclopenta[a]phenanthren-17(14H)-one

Guidance literature:: With methanol; potassium hydroxide; In dichloromethane; at 0 ℃; for 1.5h; Inert atmosphere;

Reference yield:

: 55180-24-0,130273-69-7
3,3,17,17-di(ethylenedioxy)-5,10-epoxy-estr-9⁽¹¹⁾-ene

: 1236152-98-9
(8S,9R,11S,13S,14S)-11-(4-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)phenyl)-7,8,9,11,12,13,15,16-octahydro-3-hydroxy-13-methyl-6hcyclopenta[a]phenanthren-17(14H)-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: copper(l) chloride / tetrahydrofuran / Inert atmosphere

1.2: 1 h / 20 °C / Inert atmosphere

2.1: potassium carbonate / acetonitrile / 0.08 h

2.2: 10 h / 80 °C

3.1: potassium hydroxide / methanol; hexane

With potassium carbonate; copper(l) chloride; potassium hydroxide; In tetrahydrofuran; methanol; hexane; acetonitrile; 2.2: Williamson synthesis;
DOI:10.1016/j.bmc.2012.04.041