2,3-Di(tetradecoxy)propan-1-ol

Base Information

• Chemical Name: 2,3-Di(tetradecoxy)propan-1-ol
• CAS No.: 1561-55-3
• Molecular Formula: C₃₁H₆₄O₃
• Molecular Weight: 484.847
• Hs Code.: 2909499000
• DSSTox Substance ID: DTXSID00935368
• Mol file: 1561-55-3.mol

Synonyms:1,2-di-tetradecyl-sn-glycerol;1,2-ditetradecylglycerol;2,3-bis(tetradecyloxy)-1-propanol

Chemical Property of 2,3-Di(tetradecoxy)propan-1-ol

Chemical Property:

• Vapor Pressure: 3.07E-15mmHg at 25°C
• Boiling Point: 567.5°Cat760mmHg
• Flash Point: 297°C
• PSA: 38.69000
• Density: 0.88g/cm³
• LogP: 9.78270
• XLogP3: 12.6
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 30
• Exact Mass: 484.48554590
• Heavy Atom Count: 34
• Complexity: 348

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCCCCCCOCC(CO)OCCCCCCCCCCCCCC

Technology Process of 2,3-Di(tetradecoxy)propan-1-ol

There total 15 articles about 2,3-Di(tetradecoxy)propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

1,2-dimyristyloxy-3-allyloxypropane (832722-79-9) → (±)-2,3-bis-tetradecyloxypropan-1-ol (1561-55-3)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1,3-dimethylbarbituric acid; In tetrahydrofuran; at 90 ℃; Inert atmosphere;

DOI:10.1002/cbdv.201000274

Reference yield: 90.0%

C34H68O3 → (±)-2,3-bis-tetradecyloxypropan-1-ol (1561-55-3)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; trifluoroacetic acid; In ethanol; at 85 ℃; for 16h; Inert atmosphere;

Reference yield: 80.0%

1-(2,3-di-tetradecyloxy)-propyl benzylether (150749-87-4) → (±)-2,3-bis-tetradecyloxypropan-1-ol (1561-55-3)

Guidance literature:

With hydrogen; acetic acid; palladium on activated charcoal; In ethanol; at 50 ℃; under 760 Torr;

DOI:10.1039/a700716g

upstream raw materials:

toluene-4-sulfonic acid tetradecyl ester

1-myristyl-3-trityl glycerol

1,2-bis-tetradecyloxy-3-trityloxy-propane

1-(2,3-di-tetradecyloxy)-propyl benzylether

Downstream raw materials:

N-(6-hydroxyhexyl)-N-[rac-2,3-bis(tetradecyloxy)propyl]-2-nitrobenzenesulfonamide

[rac-2,3-bis(tetradecyloxy)propyl]-N-[13-hydroxy-7-(2-nitrophenylsulfonyl)-7-azatridecyl]carbamate

N-[rac-2,3-bis(tetradecyloxy)propyl]-N-[6-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyloxy)hexyl]-2-nitrobenzenesulfonamide

[rac-2,3-bis(tetradecyloxy)propyl]-N-[13-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyloxy)-7-(2-nitrophenylsulfonyl)-7-azatridecyl]carbamate