3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-carbaldehyde

Base Information

• Chemical Name: 3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-carbaldehyde
• CAS No.: 1024005-12-6
• Molecular Formula: C₁₅H₁₂F₂N₂O
• Molecular Weight: 274.27

Synonyms:3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-carbaldehyde

Chemical Property of 3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-carbaldehyde

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Technology Process of 3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-carbaldehyde

There total 1 articles about 3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2(6),3-dien-3-ylmethanol (1024005-11-5) → 3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2(6),4-dien-5-carbaldehyde (1024005-12-6)

Guidance literature:

With dipyridinium dichromate; In dichloromethane; at 20 - 35 ℃; for 3h;

Reference yield: 51.0%

3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2(6),4-dien-5-carbaldehyde (1024005-12-6) + tert-butylamine (75-64-9) → N2-[5-(2,4-diflurophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2(6),3-dien-3-ylmethyl]-2-methyl-2-propanamine (1024003-66-4)

Guidance literature:

3-(2,4-difluorophenyl)-3,4-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,4-dien-5-carbaldehyde; tert-butylamine; In 1,2-dichloro-ethane; at 20 - 35 ℃; for 0.333333h;

With sodium tris(acetoxy)borohydride; acetic acid; In 1,2-dichloro-ethane; at 20 - 35 ℃; for 8 - 16h;

upstream raw materials:

5-(2,4-difluorophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,3-dien-3-ylmethanol

Downstream raw materials:

N₂-[5-(2,4-diflurophenyl)-4,5-diazatricyclo[5.2.1.0(2,6)]deca-2⁽⁶⁾,3-dien-3-ylmethyl]-2-methyl-2-propanamine

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