Technology Process of C31H33N7O7S2
There total 8 articles about C31H33N7O7S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: methanol / 2.75 h / 0 - 10 °C / Inert atmosphere; Large scale
2.1: ethanol; iron / 20 - 25 °C / Large scale
3.1: pyridine / acetonitrile / 25 °C / Inert atmosphere; Large scale
3.2: 3 h / 10 - 25 °C / Large scale
4.1: potassium acetate / toluene / 0.75 h / 90 °C / Inert atmosphere
4.2: 90 °C
5.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate / 1,4-dioxane; water / 0.33 h / 100 °C / Microwave irradiation
With
pyridine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; ethanol; potassium acetate; iron;
In
1,4-dioxane; methanol; water; toluene; acetonitrile;
- Guidance literature:
-
With
potassium phosphate;
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride;
In
1,4-dioxane; water;
at 100 ℃;
for 0.333333h;
Microwaves;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: pyridine / acetonitrile / 25 °C / Inert atmosphere; Large scale
1.2: 3 h / 10 - 25 °C / Large scale
2.1: potassium acetate / toluene / 0.75 h / 90 °C / Inert atmosphere
2.2: 90 °C
3.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate / 1,4-dioxane; water / 0.33 h / 100 °C / Microwave irradiation
With
pyridine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium phosphate; potassium acetate;
In
1,4-dioxane; water; toluene; acetonitrile;