C₂₃H₁₆Br₂ClNO₅

Base Information

Chemical Name:C₂₃H₁₆Br₂ClNO₅
CAS No.:1312610-61-9
Molecular Formula:C₂₃H₁₆Br₂ClNO₅
Molecular Weight:581.645
Hs Code.:

C<sub>23</sub>H<sub>16</sub>Br<sub>2</sub>ClNO<sub>5</sub>

Synonyms:C₂₃H₁₆Br₂ClNO₅

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Chemical Property of C₂₃H₁₆Br₂ClNO₅

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Technology Process of C₂₃H₁₆Br₂ClNO₅

There total 9 articles about C₂₃H₁₆Br₂ClNO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 1312611-72-5
C₂₁H₁₂Cl₃NO₅

: 1312610-61-9
C₂₃H₁₆Br₂ClNO₅

Guidance literature:: diazomethane; C₂₁H₁₂Cl₃NO₅; In diethyl ether; dichloromethane; at -5 - 20 ℃; for 1h;

With hydrogen bromide; In diethyl ether; dichloromethane; water; at -5 - 20 ℃;

Reference yield:

: 457947-61-4
4-amino-5-chloro-2-methoxy-3-nitro-benzoic acid methyl ester

: 1312610-61-9
C₂₃H₁₆Br₂ClNO₅

Guidance literature:: Multi-step reaction with 7 steps

1.1: copper(I) bromide; tert.-butylnitrite / acetonitrile / 4 h / 70 °C

2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 80 °C / Inert atmosphere

3.1: boron tribromide / dichloromethane / 2 h / -70 - -60 °C

3.2: Cooling with ice

4.1: potassium carbonate / N,N-dimethyl-formamide / 40 °C

5.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 20 °C

6.1: thionyl chloride / 2 h / Reflux

7.1: dichloromethane; diethyl ether / 1 h / -5 - 20 °C

7.2: -5 - 20 °C

With thionyl chloride; tert.-butylnitrite; lithium hydroxide monohydrate; water; boron tribromide; sodium carbonate; potassium carbonate; copper(I) bromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile; 2.1: Suzuki Coupling;

Reference yield:

: 126463-85-2
4-acetylamino-5-chloro-2-methoxy-3-nitro-benzoic acid methyl ester

: 1312610-61-9
C₂₃H₁₆Br₂ClNO₅

Guidance literature:: Multi-step reaction with 8 steps

1.1: sulfuric acid / methanol / 7 h / Reflux

2.1: copper(I) bromide; tert.-butylnitrite / acetonitrile / 4 h / 70 °C

3.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol / 80 °C / Inert atmosphere

4.1: boron tribromide / dichloromethane / 2 h / -70 - -60 °C

4.2: Cooling with ice

5.1: potassium carbonate / N,N-dimethyl-formamide / 40 °C

6.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 20 °C

7.1: thionyl chloride / 2 h / Reflux

8.1: dichloromethane; diethyl ether / 1 h / -5 - 20 °C

8.2: -5 - 20 °C

With thionyl chloride; tert.-butylnitrite; lithium hydroxide monohydrate; sulfuric acid; water; boron tribromide; sodium carbonate; potassium carbonate; copper(I) bromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; acetonitrile; 3.1: Suzuki Coupling;