1,12((4S,4S')Bis(N-4-phenyl-2-oxoazetidino))-4,9-diazododecane

Base Information

• Chemical Name: 1,12((4S,4S')Bis(N-4-phenyl-2-oxoazetidino))-4,9-diazododecane
• CAS No.: 82359-89-5
• Molecular Formula: C₂₈H₃₈N₄O₂
• Molecular Weight: 462.635
• Mol file: 82359-89-5.mol

Synonyms:1,12((4S,4S')Bis(N-4-phenyl-2-oxoazetidino))-4,9-diazododecane

Chemical Property of 1,12((4S,4S')Bis(N-4-phenyl-2-oxoazetidino))-4,9-diazododecane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,12((4S,4S')Bis(N-4-phenyl-2-oxoazetidino))-4,9-diazododecane

There total 2 articles about 1,12((4S,4S')Bis(N-4-phenyl-2-oxoazetidino))-4,9-diazododecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

1,12((4S,4S')Bis(N-4-phenyl-2-oxoazetidino))-4,9-diazododecane dihydrochloride → 1,12((4S,4S')Bis(N-4-phenyl-2-oxoazetidino))-4,9-diazododecane (82359-89-5)

Guidance literature:

With sodium hydroxide; In water; pH 12;

DOI:10.1016/S0040-4020(01)92138-6

Reference yield:

(-)-(4S,4'S)-1,12-Bis(N-4-phenyl-2-oxoazetidino)-4,9-bis-((tert)-butoxycarbonyl)-4,9-diazododecane (82359-88-4) → 1,12((4S,4S')Bis(N-4-phenyl-2-oxoazetidino))-4,9-diazododecane (82359-89-5)

Guidance literature:

With formic acid; Ambient temperature;

DOI:10.1016/S0040-4039(00)86862-8

Reference yield: 25.0%

1,12((4S,4S')Bis(N-4-phenyl-2-oxoazetidino))-4,9-diazododecane (82359-89-5) → 1,4-bis<(S)-(-)-2-oxo-4-phenyl-1,5-diazacyclooctanyl>-butane (82359-84-0,88931-15-1,88931-16-2)

Guidance literature:

In diphenylether; for 3h; Heating;

DOI:10.1016/S0040-4039(00)86862-8

upstream raw materials:

(-)-(4S,4'S)-1,12-Bis(N-4-phenyl-2-oxoazetidino)-4,9-bis-((tert)-butoxycarbonyl)-4,9-diazododecane

Downstream raw materials:

1,4-bis<(S)-(-)-2-oxo-4-phenyl-1,5-diazacyclooctanyl>-butane