(E)-4-((6-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)benzo[d]thiazol-2-yl)diazenyl)-N,N-dimethylaniline

Base Information

Chemical Name:(E)-4-((6-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)benzo[d]thiazol-2-yl)diazenyl)-N,N-dimethylaniline
CAS No.:1351287-52-9
Molecular Formula:C₂₁H₂₅FN₄O₃S
Molecular Weight:432.519
Hs Code.:

Synonyms:(E)-4-((6-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)benzo[d]thiazol-2-yl)diazenyl)-N,N-dimethylaniline

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Chemical Property of (E)-4-((6-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)benzo[d]thiazol-2-yl)diazenyl)-N,N-dimethylaniline

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Technology Process of (E)-4-((6-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)benzo[d]thiazol-2-yl)diazenyl)-N,N-dimethylaniline

There total 3 articles about (E)-4-((6-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)benzo[d]thiazol-2-yl)diazenyl)-N,N-dimethylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 1351287-50-7
(E)-2-(2-(2-((2-((4-(dimethylamino)phenyl)diazenyl)benzo[d]thiazol-6-yl)oxy)ethoxy)ethoxy)ethanol

: 1351287-52-9
(E)-4-((6-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)benzo[d]thiazol-2-yl)diazenyl)-N,N-dimethylaniline

Guidance literature:: With diethylamino-sulfur trifluoride; In 1,2-dimethoxyethane; isobutene; at 20 ℃; for 1h; Cooling with acetone-dry ice;
DOI:10.1021/ml200230e

Reference yield:

: 26278-79-5
2-amino-6-hydroxybenzothiazole

: 1351287-52-9
(E)-4-((6-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)benzo[d]thiazol-2-yl)diazenyl)-N,N-dimethylaniline

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid / 0.5 h / 0 °C

1.2: 1.5 h / 0 °C

1.3: 1 h / 0 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 7 h / 100 °C

3.1: diethylamino-sulfur trifluoride / 1,2-dimethoxyethane; isobutene / 1 h / 20 °C / Cooling with acetone-dry ice

With diethylamino-sulfur trifluoride; sulfuric acid; potassium carbonate; In 1,2-dimethoxyethane; N,N-dimethyl-formamide; isobutene;
DOI:10.1021/ml200230e

Reference yield:

: 1747-60-0
6-methoxybenzothiazol-2-ylamine

: 1351287-52-9
(E)-4-((6-(2-(2-(2-fluoroethoxy)ethoxy)ethoxy)benzo[d]thiazol-2-yl)diazenyl)-N,N-dimethylaniline

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogen bromide / 20 °C / Reflux

2.1: sulfuric acid / 0.5 h / 0 °C

2.2: 1.5 h / 0 °C

2.3: 1 h / 0 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 7 h / 100 °C

4.1: diethylamino-sulfur trifluoride / 1,2-dimethoxyethane; isobutene / 1 h / 20 °C / Cooling with acetone-dry ice

With diethylamino-sulfur trifluoride; sulfuric acid; hydrogen bromide; potassium carbonate; In 1,2-dimethoxyethane; N,N-dimethyl-formamide; isobutene;
DOI:10.1021/ml200230e