(E)-2-(2-(2-((2-((4-(dimethylamino)phenyl)diazenyl)benzo[d]thiazol-6-yl)oxy)ethoxy)ethoxy)ethanol

Base Information

Chemical Name:(E)-2-(2-(2-((2-((4-(dimethylamino)phenyl)diazenyl)benzo[d]thiazol-6-yl)oxy)ethoxy)ethoxy)ethanol
CAS No.:1351287-50-7
Molecular Formula:C₂₁H₂₆N₄O₄S
Molecular Weight:430.528
Hs Code.:

Synonyms:(E)-2-(2-(2-((2-((4-(dimethylamino)phenyl)diazenyl)benzo[d]thiazol-6-yl)oxy)ethoxy)ethoxy)ethanol

Suppliers and Price of (E)-2-(2-(2-((2-((4-(dimethylamino)phenyl)diazenyl)benzo[d]thiazol-6-yl)oxy)ethoxy)ethoxy)ethanol

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Chemical Property of (E)-2-(2-(2-((2-((4-(dimethylamino)phenyl)diazenyl)benzo[d]thiazol-6-yl)oxy)ethoxy)ethoxy)ethanol

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Technology Process of (E)-2-(2-(2-((2-((4-(dimethylamino)phenyl)diazenyl)benzo[d]thiazol-6-yl)oxy)ethoxy)ethoxy)ethanol

There total 3 articles about (E)-2-(2-(2-((2-((4-(dimethylamino)phenyl)diazenyl)benzo[d]thiazol-6-yl)oxy)ethoxy)ethoxy)ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.3%

: 5197-62-6
2-[2-(chloroethoxy)ethoxy]ethanol

: 1351287-49-4
(E)-2-((4-(dimethylamino)phenyl)diazenyl)benzo[d]thiazol-6-ol

: 1351287-50-7
(E)-2-(2-(2-((2-((4-(dimethylamino)phenyl)diazenyl)benzo[d]thiazol-6-yl)oxy)ethoxy)ethoxy)ethanol

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 7h;
DOI:10.1021/ml200230e

Reference yield:

: 1747-60-0
6-methoxybenzothiazol-2-ylamine

: 1351287-50-7
(E)-2-(2-(2-((2-((4-(dimethylamino)phenyl)diazenyl)benzo[d]thiazol-6-yl)oxy)ethoxy)ethoxy)ethanol

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen bromide / 20 °C / Reflux

2.1: sulfuric acid / 0.5 h / 0 °C

2.2: 1.5 h / 0 °C

2.3: 1 h / 0 °C

3.1: potassium carbonate / N,N-dimethyl-formamide / 7 h / 100 °C

With sulfuric acid; hydrogen bromide; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/ml200230e

Reference yield:

: 26278-79-5
2-amino-6-hydroxybenzothiazole

: 1351287-50-7
(E)-2-(2-(2-((2-((4-(dimethylamino)phenyl)diazenyl)benzo[d]thiazol-6-yl)oxy)ethoxy)ethoxy)ethanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfuric acid / 0.5 h / 0 °C

1.2: 1.5 h / 0 °C

1.3: 1 h / 0 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 7 h / 100 °C

With sulfuric acid; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/ml200230e