diethyl 6-(trichloromethyl)-1,3,5-triazine-2,4-dicarboxylate

Base Information

• Chemical Name: diethyl 6-(trichloromethyl)-1,3,5-triazine-2,4-dicarboxylate
• CAS No.: 30863-21-9
• Molecular Formula: C10H10 Cl3 N3 O4
• Molecular Weight: 342.566
• Mol file: 30863-21-9.mol

Synonyms:1,3,5-Triazine-2,4-dicarboxylicacid, 6-(trichloromethyl)-, diethyl ester (9CI); s-Triazine-2,4-dicarboxylicacid, 6-(trichloromethyl)-, diethyl ester (8CI)

Chemical Property of diethyl 6-(trichloromethyl)-1,3,5-triazine-2,4-dicarboxylate

Chemical Property:

• Vapor Pressure: 2.05E-07mmHg at 25°C
• Boiling Point: 424.5°C at 760 mmHg
• Flash Point: 210.6°C
• Density: 1.494g/cm³

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of diethyl 6-(trichloromethyl)-1,3,5-triazine-2,4-dicarboxylate

There total 2 articles about diethyl 6-(trichloromethyl)-1,3,5-triazine-2,4-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

hydrogenchloride (7647-01-0,15364-23-5) + trichloroacetonitrile (545-06-2) + ethyl cyanoformate (623-49-4) → 2,4,6-tris(trichloromethyl)-s-triazine (6542-67-2) + 2-trichloromethyl-4,6-bis(ethoxycarbonyl)-1,3,5-triazine (30863-21-9) + 2,4-bis(trichloromethyl)-6-ethoxycarbonyl-1,3,5-triazine (30863-22-0) + triethyl 1,3,5-triazine-2,4,6-tricarboxylate (898-22-6)

Guidance literature:

Reference yield:

trichloroacetonitrile (545-06-2) + ethyl cyanoformate (623-49-4) → 2-trichloromethyl-4,6-bis(ethoxycarbonyl)-1,3,5-triazine (30863-21-9)

Guidance literature:

With hydrogenchloride;

Reference yield:

2-trichloromethyl-4,6-bis(ethoxycarbonyl)-1,3,5-triazine (30863-21-9) → amino-[1,3,5]triazine-2,4-dicarboxylic acid diethyl ester (30362-18-6)

Guidance literature:

With diethyl ether; ammonia; at 0 ℃;

DOI:10.1021/ja01567a073

upstream raw materials:

trichloroacetonitrile

ethyl cyanoformate

hydrogenchloride

Downstream raw materials:

amino-[1,3,5]triazine-2,4-dicarboxylic acid diethyl ester