methyl N-[[5-[1-(4-methoxy-2-methylphenyl)-1H-pyrazol-3-yl]-2-methylphenyl]methyl]carbamate

Base Information

Chemical Name:methyl N-[[5-[1-(4-methoxy-2-methylphenyl)-1H-pyrazol-3-yl]-2-methylphenyl]methyl]carbamate
CAS No.:1604808-16-3
Molecular Formula:C₂₁H₂₃N₃O₃
Molecular Weight:365.432
Hs Code.:

Synonyms:methyl N-[[5-[1-(4-methoxy-2-methylphenyl)-1H-pyrazol-3-yl]-2-methylphenyl]methyl]carbamate

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Chemical Property of methyl N-[[5-[1-(4-methoxy-2-methylphenyl)-1H-pyrazol-3-yl]-2-methylphenyl]methyl]carbamate

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Technology Process of methyl N-[[5-[1-(4-methoxy-2-methylphenyl)-1H-pyrazol-3-yl]-2-methylphenyl]methyl]carbamate

There total 7 articles about methyl N-[[5-[1-(4-methoxy-2-methylphenyl)-1H-pyrazol-3-yl]-2-methylphenyl]methyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 27060-75-9
4-bromo-3-methylanisole

: 1604809-69-9
methyl N-[[2-methyl-5-(1H-pyrazol-3-yl)phenyl]-methyl]carbamate

: 1604808-16-3
methyl N-[[5-[1-(4-methoxy-2-methylphenyl)-1H-pyrazol-3-yl]-2-methylphenyl]methyl]carbamate

Guidance literature:: With copper(l) iodide; potassium carbonate; cis-N,N'-dimethyl-1,2-diaminocyclohexane; In 1,4-dioxane; toluene; at 110 ℃; for 40h; Inert atmosphere;

Reference yield:

: 91817-68-4
N-[(2-methylphenyl)methyl]acetamide

: 1604808-16-3
methyl N-[[5-[1-(4-methoxy-2-methylphenyl)-1H-pyrazol-3-yl]-2-methylphenyl]methyl]carbamate

Guidance literature:: Multi-step reaction with 6 steps

1: aluminum (III) chloride / dichloromethane / 0 °C / Reflux

2: sulfuric acid / water / 6 h / Reflux

3: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 - 20 °C

4: toluene / 16 h / Reflux

5: hydrazine hydrate / methanol / 16 h

6: copper(l) iodide; potassium carbonate; cis-N,N'-dimethyl-1,2-diaminocyclohexane / toluene; 1,4-dioxane / 40 h / 110 °C / Inert atmosphere

With aluminum (III) chloride; copper(l) iodide; sulfuric acid; potassium carbonate; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; cis-N,N'-dimethyl-1,2-diaminocyclohexane; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; toluene; 1: |Friedel-Crafts Acylation;

Reference yield:

: 1604809-67-7
N-[(5-acetyl-2-methylphenyl)methyl]acetamide

: 1604808-16-3
methyl N-[[5-[1-(4-methoxy-2-methylphenyl)-1H-pyrazol-3-yl]-2-methylphenyl]methyl]carbamate

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid / water / 6 h / Reflux

2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 - 20 °C

3: toluene / 16 h / Reflux

4: hydrazine hydrate / methanol / 16 h

5: copper(l) iodide; potassium carbonate; cis-N,N'-dimethyl-1,2-diaminocyclohexane / toluene; 1,4-dioxane / 40 h / 110 °C / Inert atmosphere

With copper(l) iodide; sulfuric acid; potassium carbonate; hydrazine hydrate; N-ethyl-N,N-diisopropylamine; cis-N,N'-dimethyl-1,2-diaminocyclohexane; In tetrahydrofuran; 1,4-dioxane; methanol; water; toluene;