1-{2-[6-(4,5-Dimethoxy-2-{1-[(E)-methoxyimino]-ethyl}-phenyl)-hexyl]-4,5-dimethoxy-phenyl}-ethanone O-methyl-oxime

Base Information

• Chemical Name: 1-{2-[6-(4,5-Dimethoxy-2-{1-[(E)-methoxyimino]-ethyl}-phenyl)-hexyl]-4,5-dimethoxy-phenyl}-ethanone O-methyl-oxime
• CAS No.: 57641-16-4
• Molecular Formula: C₂₈H₄₀N₂O₆
• Molecular Weight: 500.635

Synonyms:1-{2-[6-(4,5-Dimethoxy-2-{1-[(E)-methoxyimino]-ethyl}-phenyl)-hexyl]-4,5-dimethoxy-phenyl}-ethanone O-methyl-oxime

Chemical Property of 1-{2-[6-(4,5-Dimethoxy-2-{1-[(E)-methoxyimino]-ethyl}-phenyl)-hexyl]-4,5-dimethoxy-phenyl}-ethanone O-methyl-oxime

Chemical Property:

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Technology Process of 1-{2-[6-(4,5-Dimethoxy-2-{1-[(E)-methoxyimino]-ethyl}-phenyl)-hexyl]-4,5-dimethoxy-phenyl}-ethanone O-methyl-oxime

There total 2 articles about 1-{2-[6-(4,5-Dimethoxy-2-{1-[(E)-methoxyimino]-ethyl}-phenyl)-hexyl]-4,5-dimethoxy-phenyl}-ethanone O-methyl-oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,6-bis(3,4-dimethoxyphenyl)-1,6-hexanedione (50766-16-0) → 1-{2-[6-(4,5-Dimethoxy-2-{1-[(E)-methoxyimino]-ethyl}-phenyl)-hexyl]-4,5-dimethoxy-phenyl}-ethanone O-methyl-oxime (57641-16-4)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂ / Pd-C / acetic acid

2: AlCl₃

3: ethanol; pyridine

With aluminium trichloride; hydrogen; palladium on activated charcoal; In pyridine; ethanol; acetic acid;

DOI:10.1021/jm00224a002

Reference yield:

1,6-Bis-(2-acetyl-4,5-dimethoxyphenyl)-hexan (57641-14-2) + N-methoxylamine hydrochloride (593-56-6) → 1-{2-[6-(4,5-Dimethoxy-2-{1-[(E)-methoxyimino]-ethyl}-phenyl)-hexyl]-4,5-dimethoxy-phenyl}-ethanone O-methyl-oxime (57641-16-4)

Guidance literature:

In pyridine; ethanol;

DOI:10.1021/jm00224a002

Reference yield:

1-{2-[6-(4,5-Dimethoxy-2-{1-[(E)-methoxyimino]-ethyl}-phenyl)-hexyl]-4,5-dimethoxy-phenyl}-ethanone O-methyl-oxime (57641-16-4) → 1-(2-{6-[2-(1-Amino-ethyl)-4,5-dimethoxy-phenyl]-hexyl}-4,5-dimethoxy-phenyl)-ethylamine

Guidance literature:

With diborane;

DOI:10.1021/jm00224a002

upstream raw materials:

1,6-Bis-(2-acetyl-4,5-dimethoxyphenyl)-hexan

N-methoxylamine hydrochloride

1,6-bis(3,4-dimethoxyphenyl)-1,6-hexanedione

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