2-benzyl 1-(tert-butyl) (2S)-4-benzyl-5-oxo-1,2-pyrrolidinedicarboxylate

Base Information

• Chemical Name: 2-benzyl 1-(tert-butyl) (2S)-4-benzyl-5-oxo-1,2-pyrrolidinedicarboxylate
• CAS No.: 1243255-28-8
• Molecular Formula: C₂₄H₂₇NO₅
• Molecular Weight: 409.482

Synonyms:2-benzyl 1-(tert-butyl) (2S)-4-benzyl-5-oxo-1,2-pyrrolidinedicarboxylate

Chemical Property of 2-benzyl 1-(tert-butyl) (2S)-4-benzyl-5-oxo-1,2-pyrrolidinedicarboxylate

Chemical Property:

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Technology Process of 2-benzyl 1-(tert-butyl) (2S)-4-benzyl-5-oxo-1,2-pyrrolidinedicarboxylate

There total 1 articles about 2-benzyl 1-(tert-butyl) (2S)-4-benzyl-5-oxo-1,2-pyrrolidinedicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

benzyl bromide (100-39-0) + benzyl (2S)-N-tert-butoxycarbonyl-5-oxoprolinate (113400-36-5,400626-71-3) → 2-benzyl 1-(tert-butyl) (2S)-4-benzyl-5-oxo-1,2-pyrrolidinedicarboxylate (1243255-28-8)

Guidance literature:

benzyl (2S)-N-tert-butoxycarbonyl-5-oxoprolinate; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 1.08333h; Inert atmosphere;

benzyl bromide; In tetrahydrofuran; at -78 ℃; for 16.05h; stereoselective reaction; Inert atmosphere;

DOI:10.1021/jm1002556

Reference yield:

2-benzyl 1-(tert-butyl) (2S)-4-benzyl-5-oxo-1,2-pyrrolidinedicarboxylate (1243255-28-8) → C17H21NO5 (1243255-30-2)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In methanol; at 20 ℃; for 16h;

DOI:10.1021/jm1002556

upstream raw materials:

benzyl bromide

benzyl (2S)-N-tert-butoxycarbonyl-5-oxoprolinate

Downstream raw materials:

C₁₇H₂₁NO₅

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