Potassium; (1S,2R)-1-hydrazinocarbonyl-2-[3-(2-methoxy-ethoxymethoxy)-phenyl]-cyclopropanecarboxylate

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Chemical Name:Potassium; (1S,2R)-1-hydrazinocarbonyl-2-[3-(2-methoxy-ethoxymethoxy)-phenyl]-cyclopropanecarboxylate
CAS No.:139461-84-0
Molecular Formula:C₁₅H₁₉N₂O₆*K
Molecular Weight:362.424
Hs Code.:

Synonyms:Potassium; (1S,2R)-1-hydrazinocarbonyl-2-[3-(2-methoxy-ethoxymethoxy)-phenyl]-cyclopropanecarboxylate

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Chemical Property of Potassium; (1S,2R)-1-hydrazinocarbonyl-2-[3-(2-methoxy-ethoxymethoxy)-phenyl]-cyclopropanecarboxylate

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Technology Process of Potassium; (1S,2R)-1-hydrazinocarbonyl-2-[3-(2-methoxy-ethoxymethoxy)-phenyl]-cyclopropanecarboxylate

There total 5 articles about Potassium; (1S,2R)-1-hydrazinocarbonyl-2-[3-(2-methoxy-ethoxymethoxy)-phenyl]-cyclopropanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-83-4
meta-hydroxybenzaldehyde

: 139461-84-0
Potassium; (1S,2R)-1-hydrazinocarbonyl-2-[3-(2-methoxy-ethoxymethoxy)-phenyl]-cyclopropanecarboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: 70 percent / aq. NaOH, Aliquat 336 / CH₂Cl₂ / Ambient temperature

2: 89 percent / piperidine, acetic acid / toluene / Heating

3: 1.) NaH / 1.) DMSO, RT, 30 min, 2.) THF a) RT, 1 h, b) 50 - 60 deg C, 1 h

4: 95.6 percent / aq. NaOH / ethanol / 40 h / Ambient temperature

5: 1.) KOH, 2.) aq. N₂NNH₂ / 1.) EtOH, RT, 1 h, 2.) EtOH, reflux, 36 h

With piperidine; potassium hydroxide; sodium hydroxide; azido amine; Aliquat 336; sodium hydride; acetic acid; In ethanol; dichloromethane; toluene;
DOI:10.1021/jm00086a009

Reference yield:

: 139461-72-6
(3-methoxyethoxymethyloxy)benzaldehyde

: 139461-84-0
Potassium; (1S,2R)-1-hydrazinocarbonyl-2-[3-(2-methoxy-ethoxymethoxy)-phenyl]-cyclopropanecarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / piperidine, acetic acid / toluene / Heating

2: 1.) NaH / 1.) DMSO, RT, 30 min, 2.) THF a) RT, 1 h, b) 50 - 60 deg C, 1 h

3: 95.6 percent / aq. NaOH / ethanol / 40 h / Ambient temperature

4: 1.) KOH, 2.) aq. N₂NNH₂ / 1.) EtOH, RT, 1 h, 2.) EtOH, reflux, 36 h

With piperidine; potassium hydroxide; sodium hydroxide; azido amine; sodium hydride; acetic acid; In ethanol; toluene;
DOI:10.1021/jm00086a009

Reference yield:

: 139461-73-7
diethyl <3-<(2-methoxyethoxy)methoxy>benzal>malonate

: 139461-84-0
Potassium; (1S,2R)-1-hydrazinocarbonyl-2-[3-(2-methoxy-ethoxymethoxy)-phenyl]-cyclopropanecarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) DMSO, RT, 30 min, 2.) THF a) RT, 1 h, b) 50 - 60 deg C, 1 h

2: 95.6 percent / aq. NaOH / ethanol / 40 h / Ambient temperature

3: 1.) KOH, 2.) aq. N₂NNH₂ / 1.) EtOH, RT, 1 h, 2.) EtOH, reflux, 36 h

With potassium hydroxide; sodium hydroxide; azido amine; sodium hydride; In ethanol;
DOI:10.1021/jm00086a009