C₄₆H₄₉FN₆O₆

Base Information

Chemical Name:C₄₆H₄₉FN₆O₆
CAS No.:1408065-32-6
Molecular Formula:C₄₆H₄₉FN₆O₆
Molecular Weight:800.93
Hs Code.:

C<sub>46</sub>H<sub>49</sub>FN<sub>6</sub>O<sub>6</sub>

Synonyms:C₄₆H₄₉FN₆O₆

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Chemical Property of C₄₆H₄₉FN₆O₆

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Technology Process of C₄₆H₄₉FN₆O₆

There total 4 articles about C₄₆H₄₉FN₆O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1408065-30-4
C₅₀H₅₇FN₆O₆

: 1408065-32-6
C₄₆H₄₉FN₆O₆

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 1.5h; Inert atmosphere;
DOI:10.1039/c2ob26103k

Reference yield:

: 131230-76-7
4-[(tert-butyldimethylsilyloxy)methyl]aniline

: 1408065-32-6
C₄₆H₄₉FN₆O₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-ethyl-N,N-diisopropylamine; HATU / dichloromethane / 0.17 h / 20 °C / Inert atmosphere

1.2: 28 h / 20 °C / Inert atmosphere

2.1: pyridine hydrogenfluoride / tetrahydrofuran / 1.25 h / 0 °C / Inert atmosphere

3.1: manganese(IV) oxide / dichloromethane / 22 h / 20 °C / Inert atmosphere

4.1: sodium tris(acetoxy)borohydride; N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 18 h / 20 °C / Inert atmosphere

5.1: trifluoroacetic acid / dichloromethane / 1.5 h / 0 - 20 °C / Inert atmosphere

With manganese(IV) oxide; sodium tris(acetoxy)borohydride; pyridine hydrogenfluoride; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1039/c2ob26103k

Reference yield:

: 1408065-28-0
Fmoc-Glu-OtBu

: 1408065-32-6
C₄₆H₄₉FN₆O₆

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tris(acetoxy)borohydride; N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 18 h / 20 °C / Inert atmosphere

2: trifluoroacetic acid / dichloromethane / 1.5 h / 0 - 20 °C / Inert atmosphere

With sodium tris(acetoxy)borohydride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1039/c2ob26103k