N-(3-((3,5-dimethylphenyl)amino)-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-3-nitrobenzenesulfonamide

Base Information

Chemical Name:N-(3-((3,5-dimethylphenyl)amino)-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-3-nitrobenzenesulfonamide
CAS No.:1610042-58-4
Molecular Formula:C₂₄H₁₉N₃O₆S
Molecular Weight:477.497
Hs Code.:

Synonyms:N-(3-((3,5-dimethylphenyl)amino)-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-3-nitrobenzenesulfonamide

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Chemical Property of N-(3-((3,5-dimethylphenyl)amino)-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-3-nitrobenzenesulfonamide

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Technology Process of N-(3-((3,5-dimethylphenyl)amino)-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-3-nitrobenzenesulfonamide

There total 2 articles about N-(3-((3,5-dimethylphenyl)amino)-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-3-nitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 1610042-49-3
N-(3-chloro-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-3-nitrobenzenesulfonamide

: 108-69-0
3,5-dimethylaminoaniline

: 1610042-58-4
N-(3-((3,5-dimethylphenyl)amino)-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-3-nitrobenzenesulfonamide

Guidance literature:: N-(3-chloro-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-3-nitrobenzenesulfonamide; With cerium(III) chloride heptahydrate; In methanol; at 20 ℃; for 1.5h; Microwave irradiation;

3,5-dimethylaminoaniline; In methanol; at 90 ℃; for 16h; Sealed tube; Microwave irradiation;
DOI:10.1016/j.bmc.2014.03.015

Reference yield:

: 117-80-6
2,3-Dichloro-1,4-naphthoquinone

: 121-52-8
3-nitrophenylsulfonamide

: 1610042-58-4
N-(3-((3,5-dimethylphenyl)amino)-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-3-nitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 20 °C / Sealed tube; Microwave irradiation

2.1: cerium(III) chloride heptahydrate / methanol / 1.5 h / 20 °C / Microwave irradiation

2.2: 16 h / 90 °C / Sealed tube; Microwave irradiation

With cerium(III) chloride heptahydrate; caesium carbonate; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2014.03.015