N-(3-chloro-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-3-nitrobenzenesulfonamide

Base Information

• Chemical Name: N-(3-chloro-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-3-nitrobenzenesulfonamide
• CAS No.: 1610042-49-3
• Molecular Formula: C₁₆H₉ClN₂O₆S
• Molecular Weight: 392.776
• Mol file: 1610042-49-3.mol

Synonyms:N-(3-chloro-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-3-nitrobenzenesulfonamide

Chemical Property of N-(3-chloro-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-3-nitrobenzenesulfonamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(3-chloro-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-3-nitrobenzenesulfonamide

There total 1 articles about N-(3-chloro-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-3-nitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2,3-Dichloro-1,4-naphthoquinone (117-80-6) + 3-nitrophenylsulfonamide (121-52-8) → N-(3-chloro-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-3-nitrobenzenesulfonamide (1610042-49-3)

Guidance literature:

With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; Sealed tube; Microwave irradiation;

DOI:10.1016/j.bmc.2014.03.015

Reference yield: 26.0%

N-(3-chloro-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-3-nitrobenzenesulfonamide (1610042-49-3) + 3,5-dimethylaminoaniline (108-69-0) → N-(3-((3,5-dimethylphenyl)amino)-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-3-nitrobenzenesulfonamide (1610042-58-4)

Guidance literature:

N-(3-chloro-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-3-nitrobenzenesulfonamide; With cerium(III) chloride heptahydrate; In methanol; at 20 ℃; for 1.5h; Microwave irradiation;

3,5-dimethylaminoaniline; In methanol; at 90 ℃; for 16h; Sealed tube; Microwave irradiation;

DOI:10.1016/j.bmc.2014.03.015

upstream raw materials:

2,3-Dichloro-1,4-naphthoquinone

3-nitrophenylsulfonamide

Downstream raw materials:

N-(3-((3,5-dimethylphenyl)amino)-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-3-nitrobenzenesulfonamide