2-(5-(1,1,6,6-tetramethyl-10-oxo-2,3,5,6-tetrahydro-1H,4H,10H-11-oxa-3a-azabenzo[de]anthracen-9-yl)thiophene-2-yl)-3,4-ethylenedioxythiophen-5-yl-4-benzaldehyde

Base Information

Chemical Name:2-(5-(1,1,6,6-tetramethyl-10-oxo-2,3,5,6-tetrahydro-1H,4H,10H-11-oxa-3a-azabenzo[de]anthracen-9-yl)thiophene-2-yl)-3,4-ethylenedioxythiophen-5-yl-4-benzaldehyde
CAS No.:1313219-46-3
Molecular Formula:C₃₆H₃₃NO₅S₂
Molecular Weight:623.794
Hs Code.:

2-(5-(1,1,6,6-tetramethyl-10-oxo-2,3,5,6-tetrahydro-1H,4H,10H-11-oxa-3a-azabenzo[de]anthracen-9-yl)thiophene-2-yl)-3,4-ethylenedioxythiophen-5-yl-4-benzaldehyde

Synonyms:2-(5-(1,1,6,6-tetramethyl-10-oxo-2,3,5,6-tetrahydro-1H,4H,10H-11-oxa-3a-azabenzo[de]anthracen-9-yl)thiophene-2-yl)-3,4-ethylenedioxythiophen-5-yl-4-benzaldehyde

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Chemical Property of 2-(5-(1,1,6,6-tetramethyl-10-oxo-2,3,5,6-tetrahydro-1H,4H,10H-11-oxa-3a-azabenzo[de]anthracen-9-yl)thiophene-2-yl)-3,4-ethylenedioxythiophen-5-yl-4-benzaldehyde

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Technology Process of 2-(5-(1,1,6,6-tetramethyl-10-oxo-2,3,5,6-tetrahydro-1H,4H,10H-11-oxa-3a-azabenzo[de]anthracen-9-yl)thiophene-2-yl)-3,4-ethylenedioxythiophen-5-yl-4-benzaldehyde

There total 4 articles about 2-(5-(1,1,6,6-tetramethyl-10-oxo-2,3,5,6-tetrahydro-1H,4H,10H-11-oxa-3a-azabenzo[de]anthracen-9-yl)thiophene-2-yl)-3,4-ethylenedioxythiophen-5-yl-4-benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1313219-44-1
2-(5-(1,1,6,6-tetramethyl-10-oxo-2,3,5,6-tetrahydro-1H,4H,10H-11-oxa-3a-azabenzo[de]anthracen-9-yl)thiophene-2-yl)-5-bromo-3,4-ethylenedioxythiophene

: 87199-17-5
4-formylphenylboronic acid,

: 1313219-46-3
2-(5-(1,1,6,6-tetramethyl-10-oxo-2,3,5,6-tetrahydro-1H,4H,10H-11-oxa-3a-azabenzo[de]anthracen-9-yl)thiophene-2-yl)-3,4-ethylenedioxythiophen-5-yl-4-benzaldehyde

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In tetrahydrofuran; water; toluene; at 80 ℃; for 8h; Inert atmosphere;
DOI:10.1016/j.dyepig.2011.01.009

Reference yield:

: 865087-24-7
9-(5-bromothiophen-2-yl)-1,1,6,6-tetramethyl-2,3,5,6-tetrahydro-1H,4H-11-oxy-3a-azabenzo[de]anthracen-10-one

: 1313219-46-3
2-(5-(1,1,6,6-tetramethyl-10-oxo-2,3,5,6-tetrahydro-1H,4H,10H-11-oxa-3a-azabenzo[de]anthracen-9-yl)thiophene-2-yl)-3,4-ethylenedioxythiophen-5-yl-4-benzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran / 20 h / 80 °C / Inert atmosphere

2: N-Bromosuccinimide / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / tetrahydrofuran; water; toluene / 8 h / 80 °C / Inert atmosphere

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In tetrahydrofuran; water; N,N-dimethyl-formamide; toluene; 1: Stille reaction / 3: Suzuki coupling;
DOI:10.1016/j.dyepig.2011.01.009

Reference yield:

: 1313219-41-8
2-(5-(1,1,6,6-tetramethyl-10-oxo-2,3,5,6-tetrahydro-1H,4H,10H-11-oxa-3a-azabenzo[de]anthracen-9-yl)thiophene-2-yl)-3,4-ethylenedioxythiophene

: 1313219-46-3
2-(5-(1,1,6,6-tetramethyl-10-oxo-2,3,5,6-tetrahydro-1H,4H,10H-11-oxa-3a-azabenzo[de]anthracen-9-yl)thiophene-2-yl)-3,4-ethylenedioxythiophen-5-yl-4-benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / tetrahydrofuran; water; toluene / 8 h / 80 °C / Inert atmosphere

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In tetrahydrofuran; water; N,N-dimethyl-formamide; toluene; 2: Suzuki coupling;
DOI:10.1016/j.dyepig.2011.01.009