N-nitroso-2-benzylimidazoline

Base Information

• Chemical Name: N-nitroso-2-benzylimidazoline
• CAS No.: 1011736-08-5
• Molecular Formula: C₁₀H₁₁N₃O
• Molecular Weight: 189.217
• Mol file: 1011736-08-5.mol

Synonyms:N-nitroso-2-benzylimidazoline

Chemical Property of N-nitroso-2-benzylimidazoline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-nitroso-2-benzylimidazoline

There total 4 articles about N-nitroso-2-benzylimidazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

tolazoline hydrochloride (59-97-2) → N-nitroso-2-benzylimidazoline (1011736-08-5)

Guidance literature:

With hydrogenchloride; sodium nitrate; dichloromethane; In phosphate buffer; at 20 ℃; pH=4;

DOI:10.1021/tx700317g

Reference yield: 8.7%

tolazoline (59-98-3) → N-nitroso-2-benzylimidazoline (1011736-08-5) + N-nitroso-2-imidazolinyl phenyl ketoxime + 2-hydroxyethyl 2-phenylacetate (28481-53-0)

Guidance literature:

With Nitrite; for 1h; pH=3;

DOI:10.1021/tx700317g

Reference yield: 0.13%

tolazoline (59-98-3) → N-nitroso-2-benzylimidazoline (1011736-08-5)

Guidance literature:

With nitric oxide; oxygen; In phosphate buffer; at 37 ℃; for 1h; pH=7.2;

DOI:10.1021/tx700317g

upstream raw materials:

tolazoline

tolazoline hydrochloride

Downstream raw materials:

N-(1-hydroxyethyl)phenylacetamide

2-aminoethyl phenylacetate hydrochloride

N-(2-hydroxyethyl)-2-phenylacetamide

N-(2-chloroethyl)phenylacetamide