3-[4-(3,4-dimethoxyphenyl)-4-isopropyl-4-cyanobutyl]-6,7-dimethoxy-3,4-dihydroisoquinoline

Base Information

• Chemical Name: 3-[4-(3,4-dimethoxyphenyl)-4-isopropyl-4-cyanobutyl]-6,7-dimethoxy-3,4-dihydroisoquinoline
• CAS No.: 112276-31-0
• Molecular Formula: C₂₇H₃₄N₂O₄
• Molecular Weight: 450.578

Synonyms:3-[4-(3,4-dimethoxyphenyl)-4-isopropyl-4-cyanobutyl]-6,7-dimethoxy-3,4-dihydroisoquinoline

Chemical Property of 3-[4-(3,4-dimethoxyphenyl)-4-isopropyl-4-cyanobutyl]-6,7-dimethoxy-3,4-dihydroisoquinoline

Chemical Property:

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Technology Process of 3-[4-(3,4-dimethoxyphenyl)-4-isopropyl-4-cyanobutyl]-6,7-dimethoxy-3,4-dihydroisoquinoline

There total 42 articles about 3-[4-(3,4-dimethoxyphenyl)-4-isopropyl-4-cyanobutyl]-6,7-dimethoxy-3,4-dihydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4-dihydroisoquinoline (3230-65-7) + Na2 CO3 (step 1) + 1-(3,4-dimethoxyphenyl)-L-2-(formylamino)-(+/-)-6-cyano-6-(i-propyl)-6-(3,4-dimethoxyphenyl)hexane (105740-25-8,105740-26-9,112276-30-9,112276-34-3) → 3-[4-(3,4-dimethoxyphenyl)-4-isopropyl-4-cyanobutyl]-6,7-dimethoxy-3,4-dihydroisoquinoline (112276-31-0)

Guidance literature:

With trichlorophosphate; In aqueous Na₂ CO₃; diethyl ether;

Reference yield:

(3S,7S)-7-formamido-3,8-di-(3,4-dimethoxyphenyl)-2-methyl-3-octanenitrile (112276-30-9) → (S)-5-((S)-6,7-Dimethoxy-3,4-dihydro-isoquinolin-3-yl)-2-(3,4-dimethoxy-phenyl)-2-isopropyl-pentanenitrile (112276-31-0)

Guidance literature:

With trichlorophosphate; In acetonitrile; for 3h; Ambient temperature;

Reference yield:

(3S,7R)-7-formamido-3,8-di-(3,4-dimethoxyphenyl)-2-methyl-3-octanenitrile (105740-25-8) → (S)-5-((R)-6,7-Dimethoxy-3,4-dihydro-isoquinolin-3-yl)-2-(3,4-dimethoxy-phenyl)-2-isopropyl-pentanenitrile (112276-31-0)

Guidance literature:

With trichlorophosphate; In acetonitrile; for 3h; Ambient temperature;

upstream raw materials:

1-(3,4-dimethoxyphenyl)-L-2-(formylamino)-(+/-)-6-cyano-6-(i-propyl)-6-(3,4-dimethoxyphenyl)hexane

3,4-methoxycinnamic acid

3-cyano-3-(3,4-dimethoxyphenyl)-6-iodo-2-methylhexane

1-(3,4-dimethoxyphenyl)-6-cyano-6-(i-propyl)-6-(3,4-dimethoxyphenyl)hexan-2-oic acid

Downstream raw materials:

2-(3,4-Dimethoxy-phenyl)-5-(6,7-dimethoxy-1,2,3,4-tetrahydro-isoquinolin-3-yl)-2-isopropyl-pentanenitrile

(RS)-3-<(RS)-4-cyano-4-(3,4-dimethoxyphenyl)-5-methylhex-1-yl>-1,2,3,4-tetrahydro-6,7-dimethoxy-2-methylisoquinoline

(S)-2-(3,4-Dimethoxy-phenyl)-5-((S)-6,7-dimethoxy-1,2,3,4-tetrahydro-isoquinolin-3-yl)-2-isopropyl-pentanenitrile

(S)-3-<(S)-4-cyano-4-(3,4-dimethoxyphenyl)-5-methylhex-1-yl>-1,2,3,4-tetrahydro-6,7-dimethoxy-2-methylisoquinoline

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