5-(4-Thiocarbamoyl-phenyl)-2-(toluene-4-sulfonylamino)-pentanoic acid butylamide

Base Information

Chemical Name:5-(4-Thiocarbamoyl-phenyl)-2-(toluene-4-sulfonylamino)-pentanoic acid butylamide
CAS No.:83101-56-8
Molecular Formula:C₂₃H₃₁N₃O₃S₂
Molecular Weight:461.649
Hs Code.:

Synonyms:5-(4-Thiocarbamoyl-phenyl)-2-(toluene-4-sulfonylamino)-pentanoic acid butylamide

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Chemical Property of 5-(4-Thiocarbamoyl-phenyl)-2-(toluene-4-sulfonylamino)-pentanoic acid butylamide

Chemical Property:

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Technology Process of 5-(4-Thiocarbamoyl-phenyl)-2-(toluene-4-sulfonylamino)-pentanoic acid butylamide

There total 9 articles about 5-(4-Thiocarbamoyl-phenyl)-2-(toluene-4-sulfonylamino)-pentanoic acid butylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.5%

: 83116-30-7
5-(4-Cyanphenyl)-2-tosylaminovaleriansaeure-n-butylamid

: 83101-56-8
5-(4-Thiocarbamoyl-phenyl)-2-(toluene-4-sulfonylamino)-pentanoic acid butylamide

Guidance literature:: With TEA; hydrogen sulfide; In pyridine; Ambient temperature;

Reference yield:

: 35271-56-8,142917-82-6,1504-63-8
3-(4-nitrophenyl)propyl-2-en-1-ol

: 83101-56-8
5-(4-Thiocarbamoyl-phenyl)-2-(toluene-4-sulfonylamino)-pentanoic acid butylamide

Guidance literature:: Multi-step reaction with 8 steps

1: 78 percent / H₂ / Raney-Ni / methanol / 760 Torr

2: 1.) HCl/NaNO₂ / 1.) H₂O; 2.) 0-5 deg C 30 min, room temp. 4 h

3: PBr₃ / CHCl₃ / 1.5 h / Heating

4: C₂H₂ONa / ethanol / 5 h / Heating

5: 1.) 6M HCl; 2.) 1M KOH / 1.) AcOH, reflux 3 h; 2.) Et₂O, room temp. 2 h

6: SOCl₂ / 1 h / Heating

7: 73 percent / benzene / 1.5 h / Ambient temperature

8: 92.5 percent / TEA, H₂S / pyridine / Ambient temperature

With hydrogenchloride; potassium hydroxide; thionyl chloride; C₂H₂ONa; TEA; hydrogen sulfide; hydrogen; phosphorus tribromide; sodium nitrite; nickel; In pyridine; methanol; ethanol; chloroform; benzene;

Reference yield:

: 1734-79-8
3-(4-nitrophenyl)-2-propenal

: 83101-56-8
5-(4-Thiocarbamoyl-phenyl)-2-(toluene-4-sulfonylamino)-pentanoic acid butylamide

Guidance literature:: Multi-step reaction with 9 steps

1: 70 percent / NaBH₄ / methanol

2: 78 percent / H₂ / Raney-Ni / methanol / 760 Torr

3: 1.) HCl/NaNO₂ / 1.) H₂O; 2.) 0-5 deg C 30 min, room temp. 4 h

4: PBr₃ / CHCl₃ / 1.5 h / Heating

5: C₂H₂ONa / ethanol / 5 h / Heating

6: 1.) 6M HCl; 2.) 1M KOH / 1.) AcOH, reflux 3 h; 2.) Et₂O, room temp. 2 h

7: SOCl₂ / 1 h / Heating

8: 73 percent / benzene / 1.5 h / Ambient temperature

9: 92.5 percent / TEA, H₂S / pyridine / Ambient temperature

With hydrogenchloride; potassium hydroxide; sodium tetrahydroborate; thionyl chloride; C₂H₂ONa; TEA; hydrogen sulfide; hydrogen; phosphorus tribromide; sodium nitrite; nickel; In pyridine; methanol; ethanol; chloroform; benzene;