diphenylphosphine sulphide

Base Information

• Chemical Name: diphenylphosphine sulphide
• CAS No.: 55905-05-0
• Molecular Formula: C₁₂H₁₁PS
• Molecular Weight: 218.259
• Mol file: 55905-05-0.mol

Synonyms:diphenylphosphine sulphide

Chemical Property of diphenylphosphine sulphide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of diphenylphosphine sulphide

There total 2 articles about diphenylphosphine sulphide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diphenylphosphane (829-85-6) → diphenylphosphine sulphide (55905-05-0)

Guidance literature:

With sulfur; In tetrahydrofuran; for 0.5h; Schlenk technique; Inert atmosphere;

DOI:10.1080/00958972.2014.940925

Reference yield:

→ diphenylphosphine sulphide (55905-05-0)

Guidance literature:

Diphenyl-dimethylamino-phosphin, H2S, Bzl., Sd.;

DOI:10.1002/hlca.19660490406

Reference yield: 81.0%

N-benzylidene-2-(diphenylphosphino)benzeneamine (154638-80-9) + diphenylphosphine sulphide (55905-05-0) → 2-(Ph2P)C6H4NHCH(Ph)P(S)Ph2 (1271315-36-6)

Guidance literature:

In toluene; at 20 ℃; Inert atmosphere; Reflux;

DOI:10.1039/c0cc03064c

upstream raw materials:

diphenylphosphane

Downstream raw materials:

(4S)-4-benzyl-3-[(3R)-3-(diphenylphosphorothioyl)-3-phenylpropanoyl]-1,3-oxazolidin-2-one

(4S)-4-benzyl-3-[(3S)-3-(diphenylphosphorothioyl)-3-phenylpropanoyl]-1,3-oxazolidin-2-one

diphenyl(2-oxo-oxetan-2-ylmethyl)phosphine sulphide

2-(Ph₂P)C₆H₄NHCH(Ph)P(S)Ph₂