2-chloro-1-{2,5-dimethyl-1-[4-(trifluoromethoxy)phenyl]-1H-pyrrol-3-yl}-ethanone

Base Information

• Chemical Name: 2-chloro-1-{2,5-dimethyl-1-[4-(trifluoromethoxy)phenyl]-1H-pyrrol-3-yl}-ethanone
• CAS No.: 757192-82-8
• Molecular Formula: C₁₅H₁₃ClF₃NO₂
• Molecular Weight: 331.722

Synonyms:2-chloro-1-{2,5-dimethyl-1-[4-(trifluoromethoxy)phenyl]-1H-pyrrol-3-yl}-ethanone

Chemical Property of 2-chloro-1-{2,5-dimethyl-1-[4-(trifluoromethoxy)phenyl]-1H-pyrrol-3-yl}-ethanone

Chemical Property:

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Technology Process of 2-chloro-1-{2,5-dimethyl-1-[4-(trifluoromethoxy)phenyl]-1H-pyrrol-3-yl}-ethanone

There total 1 articles about 2-chloro-1-{2,5-dimethyl-1-[4-(trifluoromethoxy)phenyl]-1H-pyrrol-3-yl}-ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

2-chloro-1-{2,5-dimethyl-1-[4-(trifluoromethoxy)phenyl]-1H-pyrrol-3-yl}-ethanimine hydrochloride (1222979-13-6) → 2-chloro-1-{2,5-dimethyl-1-[4-(trifluoromethoxy)phenyl]-1H-pyrrol-3-yl}-ethanone (757192-82-8)

Guidance literature:

With water; at 100 ℃; for 1h;

DOI:10.3390/molecules15020997

Reference yield: 92.0%

2-chloro-1-{2,5-dimethyl-1-[4-(trifluoromethoxy)phenyl]-1H-pyrrol-3-yl}-ethanone (757192-82-8) + 1-methyl-5-mercaptotetrazole (13183-79-4) → 1-[2,5-dimethyl-1-(4-trifluoromethoxyphenyl)-1H-pyrrol-3-yl]-2-(1-methyl-1H-tetrazol-5-ylsulfanyl)ethanone (1222979-26-1)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 65 - 70 ℃; for 2h;

DOI:10.3390/molecules15020997

Reference yield: 89.0%

C5H5N5OS (852933-13-2) + 2-chloro-1-{2,5-dimethyl-1-[4-(trifluoromethoxy)phenyl]-1H-pyrrol-3-yl}-ethanone (757192-82-8) → 1-[2,5-dimethyl-1-(4-trifluoromethoxyphenyl)-1H-pyrrol-3-yl]-2-(5-[1,2,4]triazol-1-ylmethyl-[1,3,4]-oxadiazol-2-ylsulfanyl)ethanone (1222979-25-0)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 65 - 70 ℃; for 2h;

DOI:10.3390/molecules15020997

upstream raw materials:

2-chloro-1-{2,5-dimethyl-1-[4-(trifluoromethoxy)phenyl]-1H-pyrrol-3-yl}-ethanimine hydrochloride

Downstream raw materials:

{4-[2,5-dimethyl-1-(4-trifluoromethoxyphenyl)-1H-pyrrol-3-yl]thiazol-2-yl}-(tetrahydrofuran-2-ylmethyl)amine

4-[2,5-dimethyl-1-(4-trifluoromethoxyphenyl)-1H-pyrrol-3-yl]-2-thiophen-2-ylthiazole

1-{2-[2,5-dimethyl-1-(4-trifluoromethoxyphenyl)-1H-pyrrol-3-yl]-2-oxoethyl}-3-methylimidazolidine-2,4,5-trione

1-[2,5-dimethyl-1-(4-trifluoromethoxyphenyl)-1H-pyrrol-3-yl]-2-(5-[1,2,4]triazol-1-ylmethyl-[1,3,4]-oxadiazol-2-ylsulfanyl)ethanone

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