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5-Mercapto-1-methyltetrazole
Cas No: 13183-79-4
USD $ 3.0-3.0 / Kilogram 1 Kilogram 1-100 Metric Ton/Month Dayang Chem (Hangzhou) Co.,Ltd. Contact Supplier
High quality 1-methyl-5-mercapto-1,2,3,4-tetrazole supplier in China
Cas No: 13183-79-4
No Data 1 Kilogram 30 Metric Ton/Month Simagchem Corporation Contact Supplier
5-Mercapto-1-methyltetrazole
Cas No: 13183-79-4
No Data 1 Kilogram 20 Metric Ton/Month Henan Allgreen Chemical Co.,Ltd Contact Supplier
1-methyl-2H-tetrazole-5-thione
Cas No: 13183-79-4
No Data 10 Milligram Amadis Chemical Co., Ltd. Contact Supplier
Factory supply high quality 5-Mercapto-1-methyltetrazole 13183-79-4
Cas No: 13183-79-4
No Data No Data Metric Ton/Day Hubei Taiho Chemical Co.,LTD Contact Supplier
5-Mercapto-1-methyl-1,2,3,4-tetrazole
Cas No: 13183-79-4
No Data No Data No Data Chemwill Asia Co., Ltd. Contact Supplier
5-Mercapto-1-methyltetrazole
Cas No: 13183-79-4
USD $ 1.0-1.0 / Kilogram 1 Kilogram 1000 Metric Ton/Year Henan Sinotech Import&Export Corporation Contact Supplier
5-Mercapto-1-methyltetrazole 13183-79-4
Cas No: 13183-79-4
No Data 1 Metric Ton 10 Metric Ton/Day Henan Tianfu Chemical Co., Ltd. Contact Supplier
5-Mercapto-1-methyltetrazole CAS NO 13183-79-4
Cas No: 13183-79-4
No Data 1 Kilogram 20000 Kilogram/Day Hubei XinRunde Chemical Co., Ltd Contact Supplier
high quality 13183-79-4 5-Mercapto-1-methyltetrazole with best price
Cas No: 13183-79-4
USD $ 1.0-2.0 / Gram 10 Gram 12 Kilogram/Day Hubei Jusheng Technology Co., Ltd., Contact Supplier

13183-79-4 Usage

Uses

An impurity of Cefoperazone.

Chemical Properties

White Solid
InChI:InChI=1/C2H4N4S/c1-6-2(7)3-4-5-6/h1H3,(H,3,5,7)

13183-79-4 Well-known Company Product Price

Brand (Code)Product description CAS number Packaging Price Detail
Aldrich (357871)  5-Mercapto-1-methyltetrazole  98% 13183-79-4 357871-25G 1,173.51CNY Detail
Aldrich (357871)  5-Mercapto-1-methyltetrazole  98% 13183-79-4 357871-5G 333.45CNY Detail
Alfa Aesar (B20443)  5-Mercapto-1-methyltetrazole, 98%    13183-79-4 25g 881.0CNY Detail
Alfa Aesar (B20443)  5-Mercapto-1-methyltetrazole, 98%    13183-79-4 5g 250.0CNY Detail

13183-79-4SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 10, 2017

Revision Date: Aug 10, 2017

1.Identification

1.1 GHS Product identifier

Product name 5-Mercapto-1-methyltetrazole

1.2 Other means of identification

Product number -
Other names 1-methyl-5-mercapto-1,2,3,4-tetrazole

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:13183-79-4 SDS

13183-79-4Synthetic route

methyl thioisocyanate
556-61-6

methyl thioisocyanate

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

Conditions
ConditionsYield
With sodium azide In ethanol; water at 30 - 70℃; for 2h; Temperature; Microwave irradiation;97%
With sodium azide In ethanol at 70℃; for 3h; Cyclization;
With sodium azide for 6h; Reflux;
sodium N-methyldithiocarbamate
137-42-8

sodium N-methyldithiocarbamate

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

Conditions
ConditionsYield
With sodium azide; sodium hydroxide In water at 95℃; for 14h; Temperature;93.6%
C4H6Cl2N2S2

C4H6Cl2N2S2

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

Conditions
ConditionsYield
With sodium azide In ethanol; water at 20 - 50℃; for 2.5h;93.1%
bis (1-methyl-(1H)-tetrazol-5-yl)-disulfide
62671-38-9

bis (1-methyl-(1H)-tetrazol-5-yl)-disulfide

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

Conditions
ConditionsYield
With hydrazine In dichloromethane for 0.25h; Ambient temperature; further reagents;93%
4-methylthiosemicarbazide
6610-29-3

4-methylthiosemicarbazide

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

Conditions
ConditionsYield
Stage #1: 4-methylthiosemicarbazide With triethylamine In N,N-dimethyl-formamide; acetonitrile at 5℃; for 0.5h; Cooling with ice;
Stage #2: With n-Butyl nitrite In N,N-dimethyl-formamide; acetonitrile at 60 - 65℃; for 1h;
63%
bis (1-methyl-(1H)-tetrazol-5-yl)-disulfide
62671-38-9

bis (1-methyl-(1H)-tetrazol-5-yl)-disulfide

diluted NaOH-solution

diluted NaOH-solution

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

2-pivaloyloxymethylfuran

2-pivaloyloxymethylfuran

5-(furan-2-ylmethylthio)-1-methyl-1H-tetrazole

5-(furan-2-ylmethylthio)-1-methyl-1H-tetrazole

Conditions
ConditionsYield
With iron(III) chloride In acetonitrile at 80℃; for 0.5h;100%
thiophen-2-ylmethyl pivalate

thiophen-2-ylmethyl pivalate

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

1-methyl-5-(thiophen-2-ylmethylthio)-1H-tetrazole

1-methyl-5-(thiophen-2-ylmethylthio)-1H-tetrazole

Conditions
ConditionsYield
With iron(III) chloride In acetonitrile at 80℃; for 0.5h;100%
C20H36Au4N4O12S4

C20H36Au4N4O12S4

potassium carbonate
584-08-7

potassium carbonate

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

potassium hydroxide

potassium hydroxide

C7H10AuN5O3S2(1-)*K(1+)

C7H10AuN5O3S2(1-)*K(1+)

Conditions
ConditionsYield
In water at 20 - 80℃; for 3h;100%
1-iodo-3-phenylpropan
4119-41-9

1-iodo-3-phenylpropan

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

C11H14N4S

C11H14N4S

Conditions
ConditionsYield
In 1,4-dioxane at 110℃; for 0.25h;99%
1-naphthylmethyl 2,2-dimethylpropanoate
72681-59-5

1-naphthylmethyl 2,2-dimethylpropanoate

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

1-methyl-5-(naphthalen-1-ylmethylthio)-1H-tetrazole

1-methyl-5-(naphthalen-1-ylmethylthio)-1H-tetrazole

Conditions
ConditionsYield
With iron(III) chloride In acetonitrile at 80℃; for 0.5h;99%
(E)-3-(4-methoxyphenyl)allyl pivalate
1014394-72-9

(E)-3-(4-methoxyphenyl)allyl pivalate

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

(E)-5-(3-(4-methoxyphenyl)allylthio)-1-methyl-1H-tetrazole

(E)-5-(3-(4-methoxyphenyl)allylthio)-1-methyl-1H-tetrazole

Conditions
ConditionsYield
With iron(III) chloride In acetonitrile at 80℃; for 0.5h;99%
C18H20O2

C18H20O2

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

(E)-1-methyl-5-(3-(naphthalen-1-yl)allylthio)-1H-tetrazole

(E)-1-methyl-5-(3-(naphthalen-1-yl)allylthio)-1H-tetrazole

Conditions
ConditionsYield
With iron(III) chloride In acetonitrile at 80℃; for 1h;99%
2,3-dihydro-2H-furan
1191-99-7

2,3-dihydro-2H-furan

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

1-methyl-4-(tetrahydrofuran-2-yl)-1H-tetrazole-5(4H)-thione

1-methyl-4-(tetrahydrofuran-2-yl)-1H-tetrazole-5(4H)-thione

Conditions
ConditionsYield
In tetrahydrofuran at 65℃; for 2h;99%
1,1-Diphenylmethanol
91-01-0

1,1-Diphenylmethanol

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

1-benzhydryl-4-methyl-1,4-dihydro-5H-tetrazole-5-thione

1-benzhydryl-4-methyl-1,4-dihydro-5H-tetrazole-5-thione

Conditions
ConditionsYield
With iodine In 1,2-dichloro-ethane at 85℃; Sealed tube; chemoselective reaction;99%
1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

7-Aminocephalosporanic acid
957-68-6

7-Aminocephalosporanic acid

(6R,7R)-7-amino-3-[(1H-1-methyltetrazol-5-yl)thio]methylceph-3-em-4-carboxylic acid
24209-38-9

(6R,7R)-7-amino-3-[(1H-1-methyltetrazol-5-yl)thio]methylceph-3-em-4-carboxylic acid

Conditions
ConditionsYield
Stage #1: 1-methyl-5-mercaptotetrazole With boron trifluoride dimethyl carbonate complex; carbonic acid dimethyl ester at 10 - 12℃; for 0.166667h;
Stage #2: 7-Aminocephalosporanic acid at 25℃; for 0.75h;
Stage #3: With chloroacetyl chloride In N,N-dimethyl-formamide at 0℃; for 0.75h;
98%
With pyridine; tetrabutoxytitanium; titanium tetrachloride In acetonitrile at 5 - 30℃; for 3h; Reagent/catalyst;98%
With boron trifluoride In acetonitrile at 30℃; for 1.5h;94.7%
iodobenzene
591-50-4

iodobenzene

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

1-methyl-5-phenylthio-1,2,3,4-tetrazole

1-methyl-5-phenylthio-1,2,3,4-tetrazole

Conditions
ConditionsYield
With copper(l) iodide; 1,10-Phenanthroline; potassium carbonate In N,N-dimethyl-formamide at 120℃; for 10h;98%
With potassium phosphate; copper In dimethyl sulfoxide at 100℃; for 24h;84%
1-methyl-3-ethylimidazolium hydrogen carbonate

1-methyl-3-ethylimidazolium hydrogen carbonate

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

1-methyl-5-mercapto-1,2,3,4-tetrazole 1-methyl-3-ethylimidazolium salt

1-methyl-5-mercapto-1,2,3,4-tetrazole 1-methyl-3-ethylimidazolium salt

Conditions
ConditionsYield
In methanol for 3h;98%
1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

edaravone
89-25-8

edaravone

3-methyl-4-((1-methyl-1H-tetrazol-5-yl)thio)-1-phenyl-1H-pyrazol-5-ol

3-methyl-4-((1-methyl-1H-tetrazol-5-yl)thio)-1-phenyl-1H-pyrazol-5-ol

Conditions
ConditionsYield
With 5-ethyl-1,3,7,8-tetramethylalloxazinium triflate; iodine In acetonitrile at 25℃; under 760.051 Torr; for 24h; Green chemistry; chemoselective reaction;98%
With iodine In dimethyl sulfoxide at 80℃; for 1.5h; Green chemistry;88%
1-ethenyl-4-methylbenzene
622-97-9

1-ethenyl-4-methylbenzene

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

1-methyl-5-((1-(p-tolyl)ethyl)thio)-1H-tetrazole

1-methyl-5-((1-(p-tolyl)ethyl)thio)-1H-tetrazole

Conditions
ConditionsYield
With palladium diacetate; copper(II) bis(trifluoromethanesulfonate) In 5,5-dimethyl-1,3-cyclohexadiene at 120℃; for 4h; Inert atmosphere;97%
(E)-4-(4-fluorophenyl)but-3-en-2-ol
1092986-09-8

(E)-4-(4-fluorophenyl)but-3-en-2-ol

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

(E)-1-(4-(4-fluorophenyl)but-3-en-2-yl)-4-methyl-1,4-dihydro-5H-tetrazole-5-thione

(E)-1-(4-(4-fluorophenyl)but-3-en-2-yl)-4-methyl-1,4-dihydro-5H-tetrazole-5-thione

Conditions
ConditionsYield
With iodine In 1,2-dichloro-ethane at 85℃; Sealed tube; chemoselective reaction;97%
1,2,3-trimethoxybenzene
621-23-8

1,2,3-trimethoxybenzene

1-naphthaldehyde
66-77-3

1-naphthaldehyde

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

1-methyl-4-(naphthalen-1-yl(2,4,6-trimethoxyphenyl)methyl)-1,4-dihydro-5H-tetrazole-5-thione

1-methyl-4-(naphthalen-1-yl(2,4,6-trimethoxyphenyl)methyl)-1,4-dihydro-5H-tetrazole-5-thione

Conditions
ConditionsYield
With 2,2,2-trifluoroethanol; iodine at 20℃; for 3h; chemoselective reaction;97%
(E)-2-methyl-3-phenylallyl pivalate

(E)-2-methyl-3-phenylallyl pivalate

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

(E)-1-methyl-5-((2-methyl-3-phenylallyl)thio)-1H-tetrazole

(E)-1-methyl-5-((2-methyl-3-phenylallyl)thio)-1H-tetrazole

Conditions
ConditionsYield
With iron(III) chloride In acetonitrile at 80℃; for 1h;96%
(E)-3,7-dimethylocta-2,6-dien-1-yl pivalate
85796-37-8

(E)-3,7-dimethylocta-2,6-dien-1-yl pivalate

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

(E)-5-(3,7-dimethylocta-2,6-dienylthio)-1-methyl-1H-tetrazole

(E)-5-(3,7-dimethylocta-2,6-dienylthio)-1-methyl-1H-tetrazole

Conditions
ConditionsYield
With iron(III) chloride In acetonitrile at 80℃; for 2h;96%
acetophenone
98-86-2

acetophenone

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

2-[(1-methyl-1H-tetrazol-5-yl)sulfanyl]-1-phenylethanone
80087-27-0

2-[(1-methyl-1H-tetrazol-5-yl)sulfanyl]-1-phenylethanone

Conditions
ConditionsYield
With hydrogen iodide In water; dimethyl sulfoxide at 80℃; for 4h; Reagent/catalyst; Green chemistry; regioselective reaction;96%
With dipotassium peroxodisulfate; potassium iodide In dimethyl sulfoxide at 20℃; for 24h; Schlenk technique;85%
With dipotassium peroxodisulfate; potassium iodide In dimethyl sulfoxide at 20℃; for 24h;85%
p-methoxybenzyl 7β-(2-phenylacetamido)-3-chloromethyl-3-cephem-4-carboxylate
104146-10-3

p-methoxybenzyl 7β-(2-phenylacetamido)-3-chloromethyl-3-cephem-4-carboxylate

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

7-phenylacetylamino-3-[[(1-methyl-1H-5-tetrazolyl)thio]methyl]cephalosporanic acid p-methoxybenzyl ester

7-phenylacetylamino-3-[[(1-methyl-1H-5-tetrazolyl)thio]methyl]cephalosporanic acid p-methoxybenzyl ester

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0℃; for 10h;96%
2-(4-bromobutyl)isoindoline-1,3-dione
5394-18-3

2-(4-bromobutyl)isoindoline-1,3-dione

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

2-(4-((1-methyl-1H-tetrazol-5-yl)thio)butyl)isoindoline-1,3-dione

2-(4-((1-methyl-1H-tetrazol-5-yl)thio)butyl)isoindoline-1,3-dione

Conditions
ConditionsYield
With tetrabutylammomium bromide; potassium carbonate In N,N-dimethyl-formamide at 20℃; for 6h; Inert atmosphere;96%
(E)-1-(2-methylphenyl)-1-heptene-3-one

(E)-1-(2-methylphenyl)-1-heptene-3-one

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

(E)-4-((1-methyl-1H-tetrazol-5-yl)thio)-1-(o-tolyl)hept-1-en-3-one

(E)-4-((1-methyl-1H-tetrazol-5-yl)thio)-1-(o-tolyl)hept-1-en-3-one

Conditions
ConditionsYield
With deuterium iodide; dimethyl sulfoxide In water at 80℃; for 2.5h; regioselective reaction;96%
7β-(D-5-carboxy-5-phthalimidovaleramido)-3-(3-oxobutyryloxymethyl)-3-cephem-4-carboxylic acid

7β-(D-5-carboxy-5-phthalimidovaleramido)-3-(3-oxobutyryloxymethyl)-3-cephem-4-carboxylic acid

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

7β-(D-5-carboxy-5-phthalimidovaleramido)-3-[[(1-methyl-1H-tetrazol-5-yl)thio]methyl]ceph-3-em-4-carboxylic acid

7β-(D-5-carboxy-5-phthalimidovaleramido)-3-[[(1-methyl-1H-tetrazol-5-yl)thio]methyl]ceph-3-em-4-carboxylic acid

Conditions
ConditionsYield
With sodium bicarbonate; sodium chloride In ethyl acetate (100 ml)-water; water; toluene95.5%
1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

7-Aminocephalosporanic acid
957-68-6

7-Aminocephalosporanic acid

C10H14N6O3S2

C10H14N6O3S2

Conditions
ConditionsYield
Stage #1: 1-methyl-5-mercaptotetrazole; 7-Aminocephalosporanic acid With boron trifluoride In acetonitrile at 35 - 39℃;
Stage #2: With hydrogenchloride In water; acetonitrile at 10 - 32℃; for 0.666667h; Reagent/catalyst;
95.1%
Stage #1: 1-methyl-5-mercaptotetrazole With acetonitrile boron trifluoride complex at 30℃; for 0.5h;
Stage #2: 7-Aminocephalosporanic acid at 30℃; for 1h;
(3R,4R)-4-{(1S)-3-chloro-2-oxo-1-methylpropoxy}-3-benzamido-1-(1-diphenylmethoxycarbonyl-1-triphenylphosphoranylidenemethyl)azetidin-2-one
90244-30-7

(3R,4R)-4-{(1S)-3-chloro-2-oxo-1-methylpropoxy}-3-benzamido-1-(1-diphenylmethoxycarbonyl-1-triphenylphosphoranylidenemethyl)azetidin-2-one

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

(3R,4R)-4-{(1S)-3-(1-methyl-1H-tetrazole-5-yl)thio-2-oxo-1-methylpropoxy}-3-benzamido-1-(1-diphenylmethoxycarbonyl-1-triphenylphosphoranylidenemethyl)-azetidin-2-one
90211-61-3

(3R,4R)-4-{(1S)-3-(1-methyl-1H-tetrazole-5-yl)thio-2-oxo-1-methylpropoxy}-3-benzamido-1-(1-diphenylmethoxycarbonyl-1-triphenylphosphoranylidenemethyl)-azetidin-2-one

Conditions
ConditionsYield
In N,N-dimethyl-formamide for 1h; Ambient temperature;95%
tetramethyl ammoniumhydroxide
75-59-2

tetramethyl ammoniumhydroxide

1-methyl-5-mercaptotetrazole
13183-79-4

1-methyl-5-mercaptotetrazole

5-mercapto-1-methyltetrazole N-tetramethylammonium salt
1358553-81-7

5-mercapto-1-methyltetrazole N-tetramethylammonium salt

Conditions
ConditionsYield
In methanol at 20℃; for 12h; Inert atmosphere;95%

13183-79-4Downstream Products

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