toluene-4-sulfonic acid-(2-chloro-N-methyl-5-nitro-anilide)

Base Information

• Chemical Name: toluene-4-sulfonic acid-(2-chloro-N-methyl-5-nitro-anilide)
• CAS No.: 857005-56-2
• Molecular Formula: C₁₄H₁₃ClN₂O₄S
• Molecular Weight: 340.787
• Mol file: 857005-56-2.mol

Synonyms:toluene-4-sulfonic acid-(2-chloro-N-methyl-5-nitro-anilide)

Chemical Property of toluene-4-sulfonic acid-(2-chloro-N-methyl-5-nitro-anilide)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of toluene-4-sulfonic acid-(2-chloro-N-methyl-5-nitro-anilide)

There total 4 articles about toluene-4-sulfonic acid-(2-chloro-N-methyl-5-nitro-anilide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

toluene-4-sulfonic acid-(2-chloro-5-nitro-anilide) (346695-24-7) + methyl iodide (74-88-4) → toluene-4-sulfonic acid-(2-chloro-N-methyl-5-nitro-anilide) (857005-56-2)

Guidance literature:

With potassium carbonate; In acetone;

DOI:10.1039/b109725c

Reference yield:

N-(o-chlorophenyl)-phthalimide (22698-95-9) → toluene-4-sulfonic acid-(2-chloro-N-methyl-5-nitro-anilide) (857005-56-2)

Guidance literature:

Multi-step reaction with 3 steps

1: sulfuric acid; nitric acid / Erhitzen des Reaktionsprodukts mit wss.Natronlauge

3: aqueous NaOH-solution

With sodium hydroxide; sulfuric acid; nitric acid;

Reference yield:

H2NC6H3(Cl)NO2 (6283-25-6) → toluene-4-sulfonic acid-(2-chloro-N-methyl-5-nitro-anilide) (857005-56-2)

Guidance literature:

Multi-step reaction with 2 steps

2: aqueous NaOH-solution

With sodium hydroxide;

upstream raw materials:

toluene-4-sulfonic acid-(2-chloro-5-nitro-anilide)

dimethyl sulfate

methyl iodide

N-(o-chlorophenyl)-phthalimide

Downstream raw materials:

N₂-methyl-4-nitrobenzene-1,2-diamine

1-methyl-6-nitro-1H-benzoimidazole

2,2'-dichloro-N-methyl-5'-nitroacetanilide

2-chloro-N-methyl-5-nitro-aniline