Technology Process of C37H51NO5
There total 8 articles about C37H51NO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran; water;
at -20 ℃;
for 0.5h;
DOI:10.1021/jm900305z
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: aluminum tri-tert-butoxide; butanone / toluene / 16 h / 75 °C
1.2: 3.5 h / 20 - 49 °C
2.1: hydrogen / palladium 10% on activated carbon / pyridine / 20 °C / 760.05 Torr
3.1: triethylamine / tetrahydrofuran / 1 h / 20 °C
4.1: potassium hexamethylsilazane / tetrahydrofuran / 0.5 h / -74 °C
4.2: 0.5 h
5.1: tetrabutyl ammonium fluoride / tetrahydrofuran; water / 0.5 h / -20 °C
With
tetrabutyl ammonium fluoride; hydrogen; potassium hexamethylsilazane; aluminum tri-tert-butoxide; triethylamine; butanone;
palladium 10% on activated carbon;
In
tetrahydrofuran; pyridine; water; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogen / palladium 10% on activated carbon / pyridine / 20 °C / 760.05 Torr
2.1: triethylamine / tetrahydrofuran / 1 h / 20 °C
3.1: potassium hexamethylsilazane / tetrahydrofuran / 0.5 h / -74 °C
3.2: 0.5 h
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran; water / 0.5 h / -20 °C
With
tetrabutyl ammonium fluoride; hydrogen; potassium hexamethylsilazane; triethylamine;
palladium 10% on activated carbon;
In
tetrahydrofuran; pyridine; water;
