NC₅H₃(CNC₆H₄NCH₂C₆H₂(CH₃)3)2

Base Information

• Chemical Name: NC₅H₃(CNC₆H₄NCH₂C₆H₂(CH₃)3)2
• CAS No.: 1315594-62-7
• Molecular Formula: C₃₉H₃₇N₅
• Molecular Weight: 575.756
• Mol file: 1315594-62-7.mol

Synonyms:NC₅H₃(CNC₆H₄NCH₂C₆H₂(CH₃)3)2

Chemical Property of NC₅H₃(CNC₆H₄NCH₂C₆H₂(CH₃)3)2

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of NC₅H₃(CNC₆H₄NCH₂C₆H₂(CH₃)3)2

There total 4 articles about NC₅H₃(CNC₆H₄NCH₂C₆H₂(CH₃)3)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

2,6-bis(benzimidazole-2'-yl)pyridine (28020-73-7) + 2,4,6-trimethylbenzylbromide (4761-00-6) → NC5H3(CNC6H4NCH2C6H2(CH3)3)2 (1315594-62-7)

Guidance literature:

2,6-bis(benzimidazole-2'-yl)pyridine; With potassium hydroxide; In acetone; at 56 ℃; for 1h;

2,4,6-trimethylbenzylbromide; In acetone; for 6h; Reflux;

DOI:10.1039/c8dt03178a

Reference yield: 71.0%

2,6-bis(benzimidazole-2'-yl)pyridine (28020-73-7) + 2-chloromethyl-1,3,5-trimethylbenzene (1585-16-6) → NC5H3(CNC6H4NCH2C6H2(CH3)3)2 (1315594-62-7)

Guidance literature:

2,6-bis(benzimidazole-2'-yl)pyridine; With potassium hydroxide; In acetone; for 1h; Reflux;

2-chloromethyl-1,3,5-trimethylbenzene; In acetone; for 8h; Reflux;

DOI:10.1021/om200470p

Reference yield:

1,2-diamino-benzene (95-54-5) → NC5H3(CNC6H4NCH2C6H2(CH3)3)2 (1315594-62-7)

Guidance literature:

Multi-step reaction with 2 steps

1.1: polyphosphoric acid / 4 h / Heating

2.1: potassium hydroxide / acetone / 1 h / 56 °C

2.2: 6 h / Reflux

With potassium hydroxide; In acetone;

DOI:10.1039/c8dt03178a

upstream raw materials:

2,6-bis(benzimidazole-2'-yl)pyridine

2-chloromethyl-1,3,5-trimethylbenzene

2,4,6-trimethylbenzylbromide

1,2-diamino-benzene

Downstream raw materials:

[RuCl₂(OS(CH₃)2)(NC₅H₃(CNC₆H₄NCH₂C₆H₂(CH₃)3)2)]