methyl 4-<(3-acetamido-4-acetyl-2-propylphenoxy)methyl>-3-methoxybenzoate

Base Information

Chemical Name:methyl 4-<(3-acetamido-4-acetyl-2-propylphenoxy)methyl>-3-methoxybenzoate
CAS No.:118684-02-9
Molecular Formula:C₂₃H₂₇NO₆
Molecular Weight:413.47
Hs Code.:

Synonyms:methyl 4-<(3-acetamido-4-acetyl-2-propylphenoxy)methyl>-3-methoxybenzoate

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Chemical Property of methyl 4-<(3-acetamido-4-acetyl-2-propylphenoxy)methyl>-3-methoxybenzoate

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Technology Process of methyl 4-<(3-acetamido-4-acetyl-2-propylphenoxy)methyl>-3-methoxybenzoate

There total 7 articles about methyl 4-<(3-acetamido-4-acetyl-2-propylphenoxy)methyl>-3-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 75-36-5
acetyl chloride

: 118684-01-8
methyl 4-<(4-acetyl-3-amino-2-propylphenoxy)methyl>-3-methoxybenzoate

: 118684-02-9
methyl 4-<(3-acetamido-4-acetyl-2-propylphenoxy)methyl>-3-methoxybenzoate

Guidance literature:: With potassium carbonate; In dichloromethane; for 4h; Ambient temperature;
DOI:10.1021/jm00124a014

Reference yield:

: 42465-53-2
1-(2-amino-4-methoxyphenyl)ethanone

: 118684-02-9
methyl 4-<(3-acetamido-4-acetyl-2-propylphenoxy)methyl>-3-methoxybenzoate

Guidance literature:: Multi-step reaction with 6 steps

1: 63 percent / AlCl₃ / CH₂Cl₂ / 22 h / Ambient temperature

2: 87 percent / K₂CO₃ / acetone / 18 h / Heating

3: 54 percent / 1 h / 200 °C

4: 100 percent / H₂ / 5percent Pd/C / ethanol / 1 h / 1551.4 Torr

5: 43 percent / K₂CO₃ / acetone / 4 h / Heating

6: 67 percent / K₂CO₃ / CH₂Cl₂ / 4 h / Ambient temperature

With aluminium trichloride; hydrogen; potassium carbonate; palladium on activated charcoal; In ethanol; dichloromethane; acetone;
DOI:10.1021/jm00124a014

Reference yield:

: 536-90-3,918666-97-4
m-Anisidine

: 118684-02-9
methyl 4-<(3-acetamido-4-acetyl-2-propylphenoxy)methyl>-3-methoxybenzoate

Guidance literature:: Multi-step reaction with 7 steps

1: 1) BCl₃, 2) AlCl₃ / 1) CH₂Cl₂, -50 deg C, 30 min, 2a) -50 deg C, 1h, b) rt, 18 h, c)40 deg C, 3 h

2: 63 percent / AlCl₃ / CH₂Cl₂ / 22 h / Ambient temperature

3: 87 percent / K₂CO₃ / acetone / 18 h / Heating

4: 54 percent / 1 h / 200 °C

5: 100 percent / H₂ / 5percent Pd/C / ethanol / 1 h / 1551.4 Torr

6: 43 percent / K₂CO₃ / acetone / 4 h / Heating

7: 67 percent / K₂CO₃ / CH₂Cl₂ / 4 h / Ambient temperature

With aluminium trichloride; hydrogen; boron trichloride; potassium carbonate; palladium on activated charcoal; In ethanol; dichloromethane; acetone;
DOI:10.1021/jm00124a014