2-(Benzyloxycarbonyloxy)-3-cyclohexylamino-5,5-dimethyl-2-cyclohexen-1-on

Base Information

• Chemical Name: 2-(Benzyloxycarbonyloxy)-3-cyclohexylamino-5,5-dimethyl-2-cyclohexen-1-on
• CAS No.: 78477-02-8
• Molecular Formula: C₂₂H₂₉NO₄
• Molecular Weight: 371.477

Synonyms:2-(Benzyloxycarbonyloxy)-3-cyclohexylamino-5,5-dimethyl-2-cyclohexen-1-on

Chemical Property of 2-(Benzyloxycarbonyloxy)-3-cyclohexylamino-5,5-dimethyl-2-cyclohexen-1-on

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Technology Process of 2-(Benzyloxycarbonyloxy)-3-cyclohexylamino-5,5-dimethyl-2-cyclohexen-1-on

There total 1 articles about 2-(Benzyloxycarbonyloxy)-3-cyclohexylamino-5,5-dimethyl-2-cyclohexen-1-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

dibenzyl peroxydicarbonate (2144-45-8) + 3-Cyclohexylamino-5,5-dimethyl-2-cyclohexen-1-on (1500-76-1) → benzyl carbonochloridate (39608-52-1) + 2-(Benzyloxycarbonyloxy)-3-cyclohexylamino-5,5-dimethyl-2-cyclohexen-1-on (78477-02-8) + 2-<(Benzyloxycarbonyl)cyclohexylamino>-6-hydroxy-4,4-dimethyl-2,5-cyclohexadien-1-on (78477-07-3)

Guidance literature:

In dichloromethane; at -5 ℃;

Reference yield: 82.0%

2-(Benzyloxycarbonyloxy)-3-cyclohexylamino-5,5-dimethyl-2-cyclohexen-1-on (78477-02-8) → 3-Cyclohexylamino-2-hydroxy-5,5-dimethyl-2-cyclohexen-1-on (78476-92-3)

Guidance literature:

With hydrogen; acetic acid; palladium on activated charcoal; In ethanol; for 1h; further reagent: KOH;

Reference yield: 70.0%

2-(Benzyloxycarbonyloxy)-3-cyclohexylamino-5,5-dimethyl-2-cyclohexen-1-on (78477-02-8) → 3-Cyclohexyl-4,5-dihydro-5,5-dimethylbenzoxazol-2,7(3H,6H)-dion (78477-10-8)

Guidance literature:

With sodium hydride; In acetonitrile; at 50 - 60 ℃; further reagent: KOH;

upstream raw materials:

dibenzyl peroxydicarbonate

3-Cyclohexylamino-5,5-dimethyl-2-cyclohexen-1-on

Downstream raw materials:

3-Cyclohexylamino-2-hydroxy-5,5-dimethyl-2-cyclohexen-1-on

3-Cyclohexyl-4,5-dihydro-5,5-dimethylbenzoxazol-2,7(3H,6H)-dion

2-Cyclohexylamino-6-hydroxy-4,4-dimethyl-2,5-cyclohexadien-1-on

2-Cyclohexylamino-4,4-dimethyl-6-(4-nitrobenzoyloxy)-2,5-cyclohexadien-1-on

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