1-phenyl-5-((3-((1-phenyl-1H-tetrazol-5-yl)sulfonyl)propyl)-thio)-1H-tetrazole

Base Information

Chemical Name:1-phenyl-5-((3-((1-phenyl-1H-tetrazol-5-yl)sulfonyl)propyl)-thio)-1H-tetrazole
CAS No.:1360081-80-6
Molecular Formula:C₁₇H₁₆N₈O₂S₂
Molecular Weight:428.498
Hs Code.:

Synonyms:1-phenyl-5-((3-((1-phenyl-1H-tetrazol-5-yl)sulfonyl)propyl)-thio)-1H-tetrazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-phenyl-5-((3-((1-phenyl-1H-tetrazol-5-yl)sulfonyl)propyl)-thio)-1H-tetrazole

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Technology Process of 1-phenyl-5-((3-((1-phenyl-1H-tetrazol-5-yl)sulfonyl)propyl)-thio)-1H-tetrazole

There total 1 articles about 1-phenyl-5-((3-((1-phenyl-1H-tetrazol-5-yl)sulfonyl)propyl)-thio)-1H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 86-93-1
1-Phenyl-1H-tetrazole-5-thiol

: 717143-85-6
3-[(1-phenyl-1H-tetrazol-5-yl)sulfonyl]propan-1-ol

: 1360081-80-6
1-phenyl-5-((3-((1-phenyl-1H-tetrazol-5-yl)sulfonyl)propyl)-thio)-1H-tetrazole

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In dichloromethane; at 23 ℃; Inert atmosphere;
DOI:10.1021/jo202631e

Reference yield:

: 1360081-80-6
1-phenyl-5-((3-((1-phenyl-1H-tetrazol-5-yl)sulfonyl)propyl)-thio)-1H-tetrazole

: C₃₇H₇₂O₇Si₃

: C₄₇H₈₂N₄O₆SSi₃

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane; In tetrahydrofuran; at -78 ℃; for 1h; stereoselective reaction; Inert atmosphere;
DOI:10.1002/anie.201811093

Reference yield:

: C₁₉H₃₆O₅Si

: 1360081-80-6
1-phenyl-5-((3-((1-phenyl-1H-tetrazol-5-yl)sulfonyl)propyl)-thio)-1H-tetrazole

: C₂₉H₄₆N₄O₄SSi

: C₂₉H₄₆N₄O₄SSi

Guidance literature:: 1-phenyl-5-((3-((1-phenyl-1H-tetrazol-5-yl)sulfonyl)propyl)-thio)-1H-tetrazole; With N,N,N,N,N,N-hexamethylphosphoric triamide; potassium hexamethylsilazane; In 1,2-dimethoxyethane; toluene; at -78 ℃; for 0.5h; Inert atmosphere;

C₁₉H₃₆O₅Si; In 1,2-dimethoxyethane; toluene; at -78 ℃; for 2h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/jo202631e