methyl 2,4-di-O-benzoyl-3,6-di-O-(6-hydroxy-4-thiahexyl)-α-D-mannopyranoside

Base Information

• Chemical Name: methyl 2,4-di-O-benzoyl-3,6-di-O-(6-hydroxy-4-thiahexyl)-α-D-mannopyranoside
• CAS No.: 1001403-84-4
• Molecular Formula: C₃₁H₄₂O₁₀S₂
• Molecular Weight: 638.8

Synonyms:methyl 2,4-di-O-benzoyl-3,6-di-O-(6-hydroxy-4-thiahexyl)-α-D-mannopyranoside

Chemical Property of methyl 2,4-di-O-benzoyl-3,6-di-O-(6-hydroxy-4-thiahexyl)-α-D-mannopyranoside

Chemical Property:

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Technology Process of methyl 2,4-di-O-benzoyl-3,6-di-O-(6-hydroxy-4-thiahexyl)-α-D-mannopyranoside

There total 1 articles about methyl 2,4-di-O-benzoyl-3,6-di-O-(6-hydroxy-4-thiahexyl)-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

methyl 3,6-di-O-allyl-2,4-di-O-benzoyl-α-D-mannopyranoside (1001403-69-5) + ethanethiol (75-08-1) → methyl 2,4-di-O-benzoyl-3,6-di-O-(6-hydroxy-4-thiahexyl)-α-D-mannopyranoside (1001403-84-4)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); In 1,4-dioxane; at 75 ℃; for 4h;

DOI:10.1002/chem.200700787

Reference yield: 65.0%

O-(3,6-di-O-allyl-2,4-di-O-benzoyl-α-D-mannopyranosyl) trichloroacetimidate (1001403-75-3) + methyl 2,4-di-O-benzoyl-3,6-di-O-(6-hydroxy-4-thiahexyl)-α-D-mannopyranoside (1001403-84-4) → methyl 2,4-di-O-benzoyl-3,6-di-O-(6-[3,6-di-O-allyl-2,4-di-O-benzoyl-α-D-mannopyranosyloxy]-4-thiahexyl)-α-D-mannopyranoside (1001403-87-7)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 20 ℃;

DOI:10.1002/chem.200700787

Reference yield: 61.0%

methyl 2,4-di-O-benzoyl-3,6-di-O-(6-hydroxy-4-thiahexyl)-α-D-mannopyranoside (1001403-84-4) + 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate (183901-63-5) → methyl 2,4-di-O-benzoyl-3,6-di-O-(6-[2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyloxy]-4-thiahexyl)-α-D-mannopyranoside (1001403-85-5)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 20 ℃;

DOI:10.1002/chem.200700787

upstream raw materials:

methyl 3,6-di-O-allyl-2,4-di-O-benzoyl-α-D-mannopyranoside

ethanethiol

Downstream raw materials:

methyl 2,4-di-O-benzoyl-3,6-di-O-(6-[3,6-di-O-allyl-2,4-di-O-benzoyl-α-D-mannopyranosyloxy]-4-thiahexyl)-α-D-mannopyranoside

methyl 2,4-di-O-benzoyl-3,6-di-O-(6-[2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyloxy]-4-thiahexyl)-α-D-mannopyranoside

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