<3-(Benzyloxy)-4-methoxyphenyl>propionic acid benzyl ester

Base Information

Chemical Name:<3-(Benzyloxy)-4-methoxyphenyl>propionic acid benzyl ester
CAS No.:159749-96-9
Molecular Formula:C₂₄H₂₄O₄
Molecular Weight:376.452
Hs Code.:

Synonyms:<3-(Benzyloxy)-4-methoxyphenyl>propionic acid benzyl ester

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Chemical Property of <3-(Benzyloxy)-4-methoxyphenyl>propionic acid benzyl ester

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Technology Process of <3-(Benzyloxy)-4-methoxyphenyl>propionic acid benzyl ester

There total 3 articles about <3-(Benzyloxy)-4-methoxyphenyl>propionic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1135-15-5
dihydroisoferulic acid

: 100-39-0
benzyl bromide

: 159749-96-9
<3-(Benzyloxy)-4-methoxyphenyl>propionic acid benzyl ester

Guidance literature:: With potassium carbonate; In acetone; for 20h; Heating;
DOI:10.1021/jo00088a009

Reference yield:

: 537-73-5,1135-16-6,25522-33-2
isoferulic acid

: 159749-96-9
<3-(Benzyloxy)-4-methoxyphenyl>propionic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / H₂ / Pd/C / ethyl acetate; methanol / 5 h / 2172.02 Torr

2: K₂CO₃ / acetone; acetonitrile / 25 h / Heating

With hydrogen; potassium carbonate; palladium on activated charcoal; In methanol; ethyl acetate; acetone; acetonitrile;
DOI:10.1016/S0968-0896(03)00394-8

Reference yield:

: 621-59-0
isovanillin

: 159749-96-9
<3-(Benzyloxy)-4-methoxyphenyl>propionic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / piperidine / pyridine / 1.) 105 deg C, 3 h, 2.) 145 deg C, 1 h

2: 88 percent / H₂ / 10percent Pd-C / methanol / 12 h / Ambient temperature

3: 89 percent / K₂CO₃ / acetone / 20 h / Heating

With piperidine; hydrogen; potassium carbonate; palladium on activated charcoal; In pyridine; methanol; acetone;
DOI:10.1021/jo00088a009