tert-butyl 10-(2-(3-tert-butyl-4-methoxy-5-morpholinophenyl)-2-oxoethyl)-9-imino-2,3,5,6,10,11-hexahydro-[1,4,7]dioxazonino[2,3-f]isoindole-4(9H)-carboxylate

Base Information

Chemical Name:tert-butyl 10-(2-(3-tert-butyl-4-methoxy-5-morpholinophenyl)-2-oxoethyl)-9-imino-2,3,5,6,10,11-hexahydro-[1,4,7]dioxazonino[2,3-f]isoindole-4(9H)-carboxylate
CAS No.:1300042-69-6
Molecular Formula:C₃₄H₄₆N₄O₇
Molecular Weight:622.762
Hs Code.:

tert-butyl 10-(2-(3-tert-butyl-4-methoxy-5-morpholinophenyl)-2-oxoethyl)-9-imino-2,3,5,6,10,11-hexahydro-[1,4,7]dioxazonino[2,3-f]isoindole-4(9H)-carboxylate

Synonyms:tert-butyl 10-(2-(3-tert-butyl-4-methoxy-5-morpholinophenyl)-2-oxoethyl)-9-imino-2,3,5,6,10,11-hexahydro-[1,4,7]dioxazonino[2,3-f]isoindole-4(9H)-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl 10-(2-(3-tert-butyl-4-methoxy-5-morpholinophenyl)-2-oxoethyl)-9-imino-2,3,5,6,10,11-hexahydro-[1,4,7]dioxazonino[2,3-f]isoindole-4(9H)-carboxylate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of tert-butyl 10-(2-(3-tert-butyl-4-methoxy-5-morpholinophenyl)-2-oxoethyl)-9-imino-2,3,5,6,10,11-hexahydro-[1,4,7]dioxazonino[2,3-f]isoindole-4(9H)-carboxylate

There total 3 articles about tert-butyl 10-(2-(3-tert-butyl-4-methoxy-5-morpholinophenyl)-2-oxoethyl)-9-imino-2,3,5,6,10,11-hexahydro-[1,4,7]dioxazonino[2,3-f]isoindole-4(9H)-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 474554-48-8
2-bromo-1-[3-(tert-butyl)-4-methoxy-5-(morpholin-4-yl)phenyl]ethanone

: 1300042-68-5
C₁₇H₂₃N₃O₄

: 1300042-69-6
tert-butyl 10-(2-(3-tert-butyl-4-methoxy-5-morpholinophenyl)-2-oxoethyl)-9-imino-2,3,5,6,10,11-hexahydro-[1,4,7]dioxazonino[2,3-f]isoindole-4(9H)-carboxylate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 18h;

Reference yield:

: 300853-66-1
4,5-dihydroxyphthalonitrile

: 1300042-69-6
tert-butyl 10-(2-(3-tert-butyl-4-methoxy-5-morpholinophenyl)-2-oxoethyl)-9-imino-2,3,5,6,10,11-hexahydro-[1,4,7]dioxazonino[2,3-f]isoindole-4(9H)-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 80 °C

2: hydrogen / platinum(IV) oxide / methanol / 24 h / 20 °C

3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 18 h / 20 °C

With hydrogen; N-ethyl-N,N-diisopropylamine; triphenylphosphine; diethylazodicarboxylate; platinum(IV) oxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; 1: Mitsunobu reaction;

Reference yield:

: 103898-11-9
N,N-bis(2-hydroxyethyl)-O-tert-butylcarbamate

: 1300042-69-6
tert-butyl 10-(2-(3-tert-butyl-4-methoxy-5-morpholinophenyl)-2-oxoethyl)-9-imino-2,3,5,6,10,11-hexahydro-[1,4,7]dioxazonino[2,3-f]isoindole-4(9H)-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 80 °C

2: hydrogen / platinum(IV) oxide / methanol / 24 h / 20 °C

3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 18 h / 20 °C

With hydrogen; N-ethyl-N,N-diisopropylamine; triphenylphosphine; diethylazodicarboxylate; platinum(IV) oxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; 1: Mitsunobu reaction;