cholesteryl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranoside

Base Information

• Chemical Name: cholesteryl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranoside
• CAS No.: 141693-03-0
• Molecular Formula: C₄₁H₆₅NO₉
• Molecular Weight: 715.968
• Mol file: 141693-03-0.mol

Synonyms:cholesteryl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranoside

Chemical Property of cholesteryl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cholesteryl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranoside

There total 1 articles about cholesteryl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

cholesterol (57-88-5) + Acetic acid (2R,3S,4R,5R,6R)-3-acetoxy-2-acetoxymethyl-5-acetylamino-6-chloro-tetrahydro-pyran-4-yl ester (3068-34-6) → Cholesteryl acetate (604-35-3) + cholest-5-3-β-yl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranoside (72205-16-4) + cholesteryl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranoside (141693-03-0)

Guidance literature:

With isopropenylbenzene; at 160 ℃; for 0.3h; Yield given;

DOI:10.1016/S0040-4039(00)74174-8

Reference yield:

cholesteryl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranoside (141693-03-0) → C42H63NO6

Guidance literature:

Multi-step reaction with 2 steps

1: 82 percent / CH₃ONa, CH₃OH

2: 89 percent / H₂SO₄ / dioxane; methanol / 0.08 h / 90 - 95 °C

With methanol; sulfuric acid; sodium methylate; In 1,4-dioxane; methanol;

Reference yield:

cholesteryl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-α-D-glucopyranoside (141693-03-0) → C45H67NO8

Guidance literature:

Multi-step reaction with 3 steps

1: 82 percent / CH₃ONa, CH₃OH

2: 89 percent / H₂SO₄ / dioxane; methanol / 0.08 h / 90 - 95 °C

3: 1.) NaH / 1.) dioxane, 95 deg C, 1 h, 2.) dioxane, 65 deg C, 3 h

With methanol; sulfuric acid; sodium methylate; sodium hydride; In 1,4-dioxane; methanol;

upstream raw materials:

cholesterol

Acetic acid (2R,3S,4R,5R,6R)-3-acetoxy-2-acetoxymethyl-5-acetylamino-6-chloro-tetrahydro-pyran-4-yl ester