AcOH*H-TyrΨ(CH2O)Gly-Gly-Phe-Leu-NH2

Base Information

Chemical Name:AcOH*H-TyrΨ(CH2O)Gly-Gly-Phe-Leu-NH2
CAS No.:133851-91-9
Molecular Formula:C₂H₄O₂*C₂₈H₃₉N₅O₆
Molecular Weight:601.7
Hs Code.:

Synonyms:AcOH*H-TyrΨ(CH2O)Gly-Gly-Phe-Leu-NH2

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Chemical Property of AcOH*H-TyrΨ(CH2O)Gly-Gly-Phe-Leu-NH2

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Technology Process of AcOH*H-TyrΨ(CH2O)Gly-Gly-Phe-Leu-NH2

There total 3 articles about AcOH*H-TyrΨ(CH2O)Gly-Gly-Phe-Leu-NH2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 133851-89-5
Z-Tyr(Bzl)-Ψ(CH2O)Gly-Gly-Phe-Leu-NH2

: 64-19-7,77671-22-8
acetic acid

: 133851-91-9
AcOH*H-TyrΨ(CH2O)Gly-Gly-Phe-Leu-NH2

Guidance literature:: With ammonium formate; palladium on activated charcoal; In methanol; for 15h; Ambient temperature;
DOI:10.1021/jm00112a018

Reference yield:

: 133851-88-4
Z-Tyr(Bzl)Ψ(CH2O)Gly-OH

: 133851-91-9
AcOH*H-TyrΨ(CH2O)Gly-Gly-Phe-Leu-NH2

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) N-methylmorpholine (NMM), isobutyl chloroformate (IBCF), 2.) NMM / 1.) DMF, -25 deg C, 5 min, 2.) DMF, -20 deg C

2: 98 percent / ammonium formate / 10percent Pd/C / methanol / 15 h / Ambient temperature

With 4-methyl-morpholine; ammonium formate; isobutyl chloroformate; palladium on activated charcoal; In methanol;
DOI:10.1021/jm00112a018

Reference yield:

: 109953-94-8
Z-L-Tyr(Bzl)ψ(CH2-O)Gly-OtBu

: 133851-91-9
AcOH*H-TyrΨ(CH2O)Gly-Gly-Phe-Leu-NH2

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / trifluoroacetic acid (TFA) / CH₂Cl₂ / 1 h / Ambient temperature

2: 1.) N-methylmorpholine (NMM), isobutyl chloroformate (IBCF), 2.) NMM / 1.) DMF, -25 deg C, 5 min, 2.) DMF, -20 deg C

3: 98 percent / ammonium formate / 10percent Pd/C / methanol / 15 h / Ambient temperature

With 4-methyl-morpholine; ammonium formate; trifluoroacetic acid; isobutyl chloroformate; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1021/jm00112a018